Technology Process of 1-(3,5-dimethoxybenzyl)-3-methylbenzene
There total 3 articles about 1-(3,5-dimethoxybenzyl)-3-methylbenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; lithium chloride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 20h;
Sonication;
Inert atmosphere;
DOI:10.1016/j.ultsonch.2012.06.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride; triethylamine / dichloromethane / 2 h / Reflux; Inert atmosphere
2: zinc; ammonium chloride / benzene; diethyl ether / 12 h / 0 °C / Reflux; Inert atmosphere
3: tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; lithium chloride / N,N-dimethyl-formamide / 20 h / 20 °C / Sonication; Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); thionyl chloride; triphenyl-arsane; ammonium chloride; triethylamine; lithium chloride; zinc;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide; benzene;
3: |Stille Cross Coupling;
DOI:10.1016/j.ultsonch.2012.06.014
- Guidance literature:
-
Multi-step reaction with 2 steps
1: zinc; ammonium chloride / benzene; diethyl ether / 12 h / 0 °C / Reflux; Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; lithium chloride / N,N-dimethyl-formamide / 20 h / 20 °C / Sonication; Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; ammonium chloride; lithium chloride; zinc;
In
diethyl ether; N,N-dimethyl-formamide; benzene;
2: |Stille Cross Coupling;
DOI:10.1016/j.ultsonch.2012.06.014
