3,3-diphenyl-3H-diazirine

Base Information

• Chemical Name: 3,3-diphenyl-3H-diazirine
• CAS No.: 20188-03-8
• Molecular Formula: C₁₃H₁₀N₂
• Molecular Weight: 194.236
• Mol file: 20188-03-8.mol

Synonyms:3,3-diphenyl-3H-diazirine

Chemical Property of 3,3-diphenyl-3H-diazirine

Chemical Property:

• Boiling Point: 296.5±50.0℃ (760 Torr)
• Flash Point: 125.0±30.9℃
• Density: 1.13±0.1 g/cm3 (20 oC 760 Torr)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3-diphenyl-3H-diazirine

There total 1 articles about 3,3-diphenyl-3H-diazirine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3,3-diphenyl-3H-diazirine (20188-03-8)

Guidance literature:

Diphenyldiazomethan, Benzophenon-imin/fl. NH3, H2N-O-SO3H/Me., -70grad;

Reference yield: 29.1%

5-methoxy-2-inden-1-one (72913-59-8) + 3,3-diphenyl-3H-diazirine (20188-03-8) → 1,2-(4'-methoxybenzo)-6,6-diphenylbicyclo<3.1.0>hexan-3-one (123208-86-6)

Guidance literature:

In chloroform; benzene; 1.) 3 h, reflux, 2). 18 h, RT;

DOI:10.1021/jo00285a028

Reference yield:

3,3-diphenyl-3H-diazirine (20188-03-8) → Diphenylmethane (101-81-5)

Guidance literature:

With iodotrifluoromethane; at -270.16 ℃; Photolysis; Inert atmosphere;

DOI:10.1021/jacs.5b12726

Downstream raw materials:

diphenylmethyl (7S,6R)-7-(phenoxyacetamido)-3-{[(trifluoromethyl)sulfonyl]oxy}-1-carba-1-dethia-3-cephem-4-carboxylate

1,2-(4'-methoxybenzo)-6,6-diphenylbicyclo<3.1.0>hexan-3-one

benzhydryl (7S,6R)-7-(phenoxyacetamido)-1-carba-1-dethia-3-methyl-3-cephem-4-carboxylate

benzhydryl (7S,6R)-7-(phenoxyacetamido)-3-(methoxymethyl)-1-carba-1-dethia-3-cephem-4-carboxylate