benzyl 4-amino>butylate

Base Information

Chemical Name:benzyl 4-amino>butylate
CAS No.:158665-24-8
Molecular Formula:C₁₆H₂₃NO₅
Molecular Weight:309.362
Hs Code.:

benzyl 4-<N-<2,2-bis(hydroxymethyl)propionyl>amino>butylate

Synonyms:benzyl 4-amino>butylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 4-amino>butylate

Chemical Property:

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Technology Process of benzyl 4-amino>butylate

There total 6 articles about benzyl 4-amino>butylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: C₁₉H₂₇NO₅

: 158665-24-8
benzyl 4-amino>butylate

Guidance literature:: With acetic acid; In water; at 20 ℃; for 6h;
DOI:10.1016/j.tetlet.2015.10.084

Reference yield: 63.0%

: 4767-03-7
2,2-bis(hydroxymethyl)propionic acid

: 46347-99-3
benzyl 4-aminobutanoate

: 158665-24-8
benzyl 4-amino>butylate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1021/jo9611780

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 158665-24-8
benzyl 4-amino>butylate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / Dean-Stark; Reflux

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C

3: acetic acid / water / 6 h / 20 °C

With dmap; acetic acid; dicyclohexyl-carbodiimide; In dichloromethane; water; toluene; 1: |Fischer-Speier Esterification;
DOI:10.1016/j.tetlet.2015.10.084