C₄₁H₅₂O₆Si

Base Information

Chemical Name:C₄₁H₅₂O₆Si
CAS No.:1413373-99-5
Molecular Formula:C₄₁H₅₂O₆Si
Molecular Weight:668.946
Hs Code.:

C<sub>41</sub>H<sub>52</sub>O<sub>6</sub>Si

Synonyms:C₄₁H₅₂O₆Si

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Chemical Property of C₄₁H₅₂O₆Si

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Technology Process of C₄₁H₅₂O₆Si

There total 11 articles about C₄₁H₅₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1147490-71-8
2,3,4,6-tetra-O-benzyl-1-O-(tert-butyldimethylsilyl)-5a-carba-β-D-xylo-hex-5(5a)-enopyranose

: 1413373-99-5
C₄₁H₅₂O₆Si

Guidance literature:: 2,3,4,6-tetra-O-benzyl-1-O-(tert-butyldimethylsilyl)-5a-carba-β-D-xylo-hex-5(5a)-enopyranose; With dimethylsulfide borane complex; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1413373-99-5
C₄₁H₅₂O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

5.2: 0.75 h

6.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

6.2: 12 h / 40 °C

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 2 h / 0 - 20 °C

With pyridine; 1H-imidazole; oxalyl dichloride; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; dimethyl sulfoxide; L-proline; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 13096-62-3
(3R,4S,5R,6R)-3,4,5-tris(benzyloxy)-6-((benzyloxy)methyl)tetrahydro-2H-pyran-2-one

: 1413373-99-5
C₄₁H₅₂O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: -78 - 0 °C

1.3: cooling with ice

2.1: sodium tetrahydroborate / tetrahydrofuran / 20 °C

3.1: trifluoroacetic anhydride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C

3.2: -78 - 0 °C

4.1: potassium carbonate / 18-crown-6 ether / toluene / 20 °C

5.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

5.2: 0.75 h

6.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

6.2: 12 h / 40 °C

7.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.2: 2 h / 0 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; n-butyllithium; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride; 18-crown-6 ether; In tetrahydrofuran; methanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;