dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate

Base Information

Chemical Name:dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate
CAS No.:1146950-84-6
Molecular Formula:C₁₉H₂₀N₂O₄
Molecular Weight:340.379
Hs Code.:

Synonyms:dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate

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Chemical Property of dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate

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Technology Process of dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate

There total 1 articles about dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1072925-96-2
dimethyl 4-formyl-pyridine-2,6-dicarboxylate

: 34904-03-5
4-(N,N-dimethylamino)benzyltriphenylphosphonium iodide

: 1146950-84-6
dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere; Cooling with ice;
DOI:10.1016/j.tetlet.2008.09.073

Reference yield:

: 1146950-84-6
dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate

: C₁₇H₁₄N₂O₄^(2-)*2Na⁽¹⁺⁾

Guidance literature:: With water; sodium hydroxide; In tetrahydrofuran; at 80 ℃; for 12h;
DOI:10.1016/j.saa.2011.09.036

Reference yield:

: 1146950-84-6
dimethyl 4-[trans-4'-(N,N-dimethylamino)-styryl]pyridine-2,6-dicarboxylate

: 1345544-84-4
trans-4-(4'-(dimethylamino)styryl)pyridine-2,6-dicarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / tetrahydrofuran / 12 h / 80 °C

2: hydrogenchloride / water / 2 h / 20 °C / pH 2

With hydrogenchloride; water; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.saa.2011.09.036