6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione

Base Information

• Chemical Name: 6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione
• CAS No.: 122822-62-2
• Molecular Formula: C₃₂H₂₂N₄O₄
• Molecular Weight: 526.551

Synonyms:6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione

Chemical Property of 6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione

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Technology Process of 6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione

There total 3 articles about 6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.9%

4-(phenylazo)-1,2-naphthalenediol (122822-61-1) → 6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione (122822-62-2)

Guidance literature:

With sodium hydroxide; silver nitrate; In tetrahydrofuran; water; for 0.0833333h;

DOI:10.1021/jo00280a056

Reference yield:

dianilunium sulphate (542-16-5,2424-53-5,20305-50-4,29961-02-2) → 6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione (122822-62-2)

Guidance literature:

Multi-step reaction with 2 steps

2: 36.9 percent / AgNO₃, 1 N NaOH / tetrahydrofuran; H₂O / 0.08 h

With sodium hydroxide; silver nitrate; In tetrahydrofuran; water;

DOI:10.1021/jo00280a056

Reference yield:

1,2-naphthoquinone (524-42-5) → 6a,13a-Dihydroxy-6,13-diphenyl-6,6a,13,13a,13b,13c-hexahydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione (122822-62-2)

Guidance literature:

Multi-step reaction with 2 steps

2: 36.9 percent / AgNO₃, 1 N NaOH / tetrahydrofuran; H₂O / 0.08 h

With sodium hydroxide; silver nitrate; In tetrahydrofuran; water;

DOI:10.1021/jo00280a056

upstream raw materials:

4-(phenylazo)-1,2-naphthalenediol

dianilunium sulphate

1,2-naphthoquinone

Downstream raw materials:

6,13-Diphenyl-6,13-dihydro-5,6,12,13-tetraaza-dibenzo[b,def]chrysene-7,14-dione

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