N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

Base Information

• Chemical Name: N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide
• CAS No.: 166818-07-1
• Molecular Formula: C₂₇H₃₂I₃N₃O₁₂
• Molecular Weight: 971.277

Synonyms:N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

Chemical Property of N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

Chemical Property:

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Technology Process of N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide

There total 2 articles about N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

allyloxyacetyl chloride (56680-79-6) + N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-amino-2,4,6-triiodo-1,3-benzenedicarboxamide (148051-08-5) → N,N'-Bis[2-Hydroxy-1-(hydroxymethyl)ethyl-5-[3-(hydroxymethyl) -5-oxo-4-morpholinyl]-2,4,6-triiodo-1,3-benzenedicarboxamide + N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide (166818-07-1)

Guidance literature:

In ice-water; N,N-dimethyl acetamide;

Reference yield:

allyloxyacetyl chloride (56680-79-6) + N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-amino-2,4,6-triiodo-1,3-benzenedicarboxamide (148051-08-5) → N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide (166818-07-1)

Guidance literature:

In N,N-dimethyl acetamide; Yield given; 1.) 5 deg C, 0.5 h, 2.) room temp., 20 h;

DOI:10.1021/jo00119a020

Reference yield:

N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<<(2-propenyloxy)acetyl>amino>-2,4,6-triiodo-1,3-benzenedicarboxamide (166818-07-1) → 5-(2-Allyloxy-acetylamino)-N,N'-bis-(2-hydroxy-1-hydroxymethyl-ethyl)-2,4,6-triiodo-isophthalamide

Guidance literature:

With sodium methylate; In methanol; for 4h;

DOI:10.1021/jo00119a020

upstream raw materials:

allyloxyacetyl chloride

N,N'-bis[2-(acetyloxy)-1-[(acetyloxy)methyl]ethyl]-5-amino-2,4,6-triiodo-1,3-benzenedicarboxamide

Downstream raw materials:

N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-2,4,6-triiodo-5-<3-(iodomethyl)-5-oxo-4-morpholinyl>-1,3-benzenedicarboxamide

N,N'-Bis<2-(acetyloxy)-1-<(acetyloxy)methyl>ethyl>-5-<3-<(acetyloxy)methyl>-5-oxo-4-morpholinyl>-2,4,6-triiodo-1,3-benzenedicarboxamide

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