5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide

Base Information

Chemical Name:5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide
CAS No.:133992-54-8
Molecular Formula:C₁₃H₁₇N₅O₄
Molecular Weight:307.309
Hs Code.:

Synonyms:5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide

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Chemical Property of 5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide

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Technology Process of 5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide

There total 3 articles about 5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 133992-56-0
5-(azidomethyl)-1,2,3-trimethoxybenzene

: 107-91-5
cyanoacetic acid amide

: 133992-54-8
5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; for 24h; Ambient temperature;

Reference yield:

: 3840-31-1
(3,4,5-trimethoxyphenyl)methanol

: 133992-54-8
5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / dimethylformamide / 20 - 30 °C

2: NaN₃, 20N NH₄OH / dimethylformamide; dimethylsulfoxide / 18 h / Ambient temperature; pH 8

3: 91 percent / K₂CO₃ / dimethylsulfoxide / 24 h / Ambient temperature

With ammonium hydroxide; thionyl chloride; sodium azide; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 3840-30-0
5-(chloromethyl)-1,2,3-trimethoxybenzene

: 133992-54-8
5-Amino-1-(3,4,5-trimethoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: NaN₃, 20N NH₄OH / dimethylformamide; dimethylsulfoxide / 18 h / Ambient temperature; pH 8

2: 91 percent / K₂CO₃ / dimethylsulfoxide / 24 h / Ambient temperature

With ammonium hydroxide; sodium azide; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;