4-(Trifluoromethyl)phenylcarbothioic acid hydrazide

Base Information

Chemical Name:4-(Trifluoromethyl)phenylcarbothioic acid hydrazide
CAS No.:109684-16-4
Molecular Formula:C₈H₇F₃N₂S
Molecular Weight:220.218
Hs Code.:

Synonyms:4-(Trifluoromethyl)phenylcarbothioic acid hydrazide

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Chemical Property of 4-(Trifluoromethyl)phenylcarbothioic acid hydrazide

Chemical Property:

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Technology Process of 4-(Trifluoromethyl)phenylcarbothioic acid hydrazide

There total 1 articles about 4-(Trifluoromethyl)phenylcarbothioic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72115-97-0
[((4-(Trifluoromethyl)phenyl)thioxomethyl)thio]acetic acid

: 109684-16-4
4-(Trifluoromethyl)phenylcarbothioic acid hydrazide

Guidance literature:: With potassium hydroxide; hydrazine hydrate; In methanol; water; acetic acid;

Reference yield:

: 52709-42-9
benzylglyoxylate

: 109684-16-4
4-(Trifluoromethyl)phenylcarbothioic acid hydrazide

: benzyl 2,3-dihydro-5-[4-(trifluoromethyl)phenyl]-1,3,4-thiadiazole-2-carboxylate

Guidance literature:: In ethanol;

Reference yield:

: 109684-16-4
4-(Trifluoromethyl)phenylcarbothioic acid hydrazide

: 109683-75-2
2,3-Dihydro-3-(3-mercapto-1-oxopropyl)-5-[4-(trifluoromethyl)phenyl]-1,3,4-thiadiazole-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 16 h / Ambient temperature

2: polyvinylpyridine / toluene / 16 h / Ambient temperature

3: aq. KOH / methanol / 2 h / 10 °C

With potassium hydroxide; polyvinylpyridine; In methanol; ethanol; toluene;
DOI:10.1021/jm00105a066