N₄-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine

Base Information

• Chemical Name: N₄-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine
• CAS No.: 1043963-01-4
• Molecular Formula: C₃₉H₃₉N₃O₇Se
• Molecular Weight: 740.715

Synonyms:N₄-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine

Chemical Property of N₄-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine

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Technology Process of N₄-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine

There total 1 articles about N₄-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C18H21N3O5Se + 4,4'-dimethoxytrityl chloride (40615-36-9) → N4-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine (1043963-01-4)

Guidance literature:

In pyridine; at 20 ℃;

DOI:10.1021/ja802177u

Reference yield: 70.0%

2-cyanoethyl-N,N-diisopropylchlorophosphoramidite (100345-53-7) + N4-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine (1043963-01-4) → N4-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite (1043963-02-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/ja802177u

upstream raw materials:

4,4'-dimethoxytrityl chloride

Downstream raw materials:

N₄-acetyl-5'-O-(4,4'-dimethoxytriphenylmethyl)-5-phenylselenylmethyl-2'-deoxycytidine 3'-(2-cyanoethyl)-N,N-diisopropylphosphoramidite

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