1H-Indole-2-carboxylic acid, 1-[(4-methylphenyl)sulfonyl]-, ethyl ester

Base Information

Chemical Name:1H-Indole-2-carboxylic acid, 1-[(4-methylphenyl)sulfonyl]-, ethyl ester
CAS No.:132819-92-2
Molecular Formula:C₁₈H₁₇NO₄S
Molecular Weight:343.403
Hs Code.:
Mol file:132819-92-2.mol

Synonyms:1-(toluene-4-sulfonyl)-1H-indole-2-carboxylic acid ethyl ester

Suppliers and Price of 1H-Indole-2-carboxylic acid, 1-[(4-methylphenyl)sulfonyl]-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

DC Chemicals
NOD-IN-1 >98%
1 g
$ 1800.00

DC Chemicals
NOD-IN-1 >98%
100 mg
$ 500.00

CSNpharm
NOD-IN-1
5mg
$ 173.00

CSNpharm
NOD-IN-1
25mg
$ 497.00

CSNpharm
NOD-IN-1
50mg
$ 845.00

ChemScene
NOD-IN-1 99.60%
100mg
$ 1560.00

ChemScene
NOD-IN-1 99.60%
50mg
$ 1056.00

ChemScene
NOD-IN-1 99.60%
10mg
$ 336.00

ChemScene
NOD-IN-1 99.60%
5mg
$ 216.00

ChemScene
NOD-IN-1 99.60%
1mg
$ 108.00

Total 11 raw suppliers

Chemical Property of 1H-Indole-2-carboxylic acid, 1-[(4-methylphenyl)sulfonyl]-, ethyl ester

Chemical Property:

Melting Point:98-99 °C
Boiling Point:523.3±52.0 °C(Predicted)
Density:1.27±0.1 g/cm3(Predicted)
Storage Temp.:2-8°C

Purity/Quality:

95% ^*data from raw suppliers

NOD-IN-1 >98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1H-Indole-2-carboxylic acid, 1-[(4-methylphenyl)sulfonyl]-, ethyl ester

There total 7 articles about 1H-Indole-2-carboxylic acid, 1-[(4-methylphenyl)sulfonyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 3770-50-1,117770-52-2
2-carbethoxyindole

: 98-59-9
p-toluenesulfonyl chloride

: 132819-92-2
1-(toluene-4-sulfonyl)-1H-indole-2-carboxylic acid ethyl ester

Guidance literature:: 2-carbethoxyindole; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.0833333h; Inert atmosphere;

p-toluenesulfonyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.3762/bjoc.17.101

Reference yield: 63.0%

: ethyl (Z)-2-((4-methylphenyl)sulfonamido)-3-phenylacrylate

: 132819-92-2
1-(toluene-4-sulfonyl)-1H-indole-2-carboxylic acid ethyl ester

Guidance literature:: With Oxone; palladium diacetate; In acetic acid; N,N-dimethyl-formamide; at 80 ℃; for 15h; Reagent/catalyst; Solvent; Concentration; Time; Temperature;
DOI:10.5012/bkcs.2014.35.9.2611

Reference yield: 60.0%

: ethyl 3-(2-chlorophenyl)-1-tosylaziridine-2-carboxylate

: 132819-92-2
1-(toluene-4-sulfonyl)-1H-indole-2-carboxylic acid ethyl ester

Guidance literature:: ethyl 3-(2-chlorophenyl)-1-tosylaziridine-2-carboxylate; With boron trifluoride diethyl etherate; thiophenol; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

With copper; In dichloromethane; N,N-dimethyl-formamide; at 125 ℃; for 20h; Inert atmosphere;
DOI:10.1021/acs.joc.5b02251