1-O-oleoyl-2-O-methyl-rac-glycerol

Base Information

• Chemical Name: 1-O-oleoyl-2-O-methyl-rac-glycerol
• CAS No.: 213738-56-8
• Molecular Formula: C₂₂H₄₂O₄
• Molecular Weight: 370.573

Synonyms:1-O-oleoyl-2-O-methyl-rac-glycerol

Chemical Property of 1-O-oleoyl-2-O-methyl-rac-glycerol

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 1-O-oleoyl-2-O-methyl-rac-glycerol

There total 2 articles about 1-O-oleoyl-2-O-methyl-rac-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-monooleoyl glycerol (111-03-5,2716-53-2,30836-40-9,34487-30-4,69483-90-5,99297-71-9,129784-87-8,33978-07-3,925-14-4) → 1-O-oleoyl-2-O-methyl-rac-glycerol (213738-56-8)

Guidance literature:

Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane / 17 h / 20 °C

2: tetrafluoroboric acid / hexane; dichloromethane / 2.5 h / 0 - 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With dmap; tetrafluoroboric acid; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; hexane; dichloromethane;

DOI:10.1039/b9nj00704k

Reference yield:

→ 1-O-oleoyl-2-O-methyl-rac-glycerol (213738-56-8) + 1-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-3-(phenylmethoxy)-2-propanol (154458-56-7)

Guidance literature:

Reference yield:

1-O-oleoyl-2-O-methyl-rac-glycerol (213738-56-8) + triethylamine sulfur trioxide (761-01-3,54381-28-1) → 3-O-oleoyl-2-O-methyl-rac-glycero-1-sulfate triethylamine salt

Guidance literature:

1-O-oleoyl-2-O-methyl-rac-glycerol; triethylamine sulfur trioxide; In N,N-dimethyl-formamide; at 40 ℃; for 5.5h;

With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 0.5h;

upstream raw materials:

1-monooleoyl glycerol

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