3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid

Base Information

Chemical Name:3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid
CAS No.:1345614-66-5
Molecular Formula:C₁₉H₂₂N₄O₆S
Molecular Weight:434.473
Hs Code.:

Synonyms:3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid

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Chemical Property of 3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid

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Technology Process of 3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid

There total 4 articles about 3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1201771-20-1
3-(7-methoxy-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid

: 456-27-9
4-nitrobenzenediazonium tetrafluoroborate

: 1345614-66-5
3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid

Guidance literature:: With sulfuric acid; In methanol; at 20 ℃; for 1h;
DOI:10.1021/ol202619f

Reference yield:

: 19500-61-9
7-methoxy-1,2,3,4-tetrahydroquinoline

: 1345614-66-5
3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 20 °C

2: sulfuric acid / methanol / 1 h / 20 °C

With sulfuric acid; In methanol;
DOI:10.1021/ol202619f

Reference yield:

: 22246-17-9
7-methoxy-2-oxo-1,2,3,4-tetrahydroquinoline

: 1345614-66-5
3-(7-methoxy-6-(4-nitrophenylazo)-3,4-dihydro-2H-quinolin-1-yl)propane-1-sulfonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: borane-THF / tetrahydrofuran / Reflux

2: methanol / 20 °C

3: sulfuric acid / methanol / 1 h / 20 °C

With borane-THF; sulfuric acid; In tetrahydrofuran; methanol;
DOI:10.1021/ol202619f