(C₄H₂NCC₆H₃(C₄H₉)2)3(C₄H₂NCC₆H₃(O(CH₂)2O(CH₂)2OC₆H₄)2C₁₂H₆N₂)Au⁽¹⁺⁾*PF₆^(1-) = [C₁₀₀H₁₀₄N₆O₆Au][PF₆]

Base Information

• Chemical Name: (C₄H₂NCC₆H₃(C₄H₉)2)3(C₄H₂NCC₆H₃(O(CH₂)2O(CH₂)2OC₆H₄)2C₁₂H₆N₂)Au⁽¹⁺⁾*PF₆^(1-) = [C₁₀₀H₁₀₄N₆O₆Au][PF₆]
• CAS No.: 184959-62-4
• Molecular Formula: C₁₀₀H₁₀₄AuN₆O₆*F₆P
• Molecular Weight: 1827.89

Synonyms:(C₄H₂NCC₆H₃(C₄H₉)2)3(C₄H₂NCC₆H₃(O(CH₂)2O(CH₂)2OC₆H₄)2C₁₂H₆N₂)Au⁽¹⁺⁾*PF₆^(1-) = [C₁₀₀H₁₀₄N₆O₆Au][PF₆]

Chemical Property of (C₄H₂NCC₆H₃(C₄H₉)2)3(C₄H₂NCC₆H₃(O(CH₂)2O(CH₂)2OC₆H₄)2C₁₂H₆N₂)Au⁽¹⁺⁾*PF₆^(1-) = [C₁₀₀H₁₀₄N₆O₆Au][PF₆]

Chemical Property:

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Technology Process of (C₄H₂NCC₆H₃(C₄H₉)2)3(C₄H₂NCC₆H₃(O(CH₂)2O(CH₂)2OC₆H₄)2C₁₂H₆N₂)Au⁽¹⁺⁾*PF₆^(1-) = [C₁₀₀H₁₀₄N₆O₆Au][PF₆]

There total 3 articles about (C₄H₂NCC₆H₃(C₄H₉)2)3(C₄H₂NCC₆H₃(O(CH₂)2O(CH₂)2OC₆H₄)2C₁₂H₆N₂)Au⁽¹⁺⁾*PF₆^(1-) = [C₁₀₀H₁₀₄N₆O₆Au][PF₆] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

potassium hexafluorophosphate (17084-13-8) + potassium tetrachloroaurate(III) (13682-61-6) + (C4H2NCC6H3(C4H9)2)3(C4H2NCC6H3(O(CH2)2O(CH2)2OC6H4)2C12H6N2)H2 → (C4H2NCC6H3(C4H9)2)3(C4H2NCC6H3(O(CH2)2O(CH2)2OC6H4)2C12H6N2)Au(1+)*PF6(1-) = [C100H104N6O6Au][PF6] (184959-62-4)

Guidance literature:

With sodium acetate; In acetic acid; (Ar); refluxing, stirring (12 h); solvent removal (vac.), CH2Cl2 - aq. NaHCO3 partitioning, org. layer washing (aq. NaHCO3), conversion to hexafluorophosphate, org. layer washing(H2O), drying (Na2SO4), filtn., solvent removal, chromy. (silica, 0.5% MeOH in CH2Cl2);

DOI:10.1039/a708756j

Reference yield: 47.0%

potassium hexafluorophosphate (17084-13-8) + potassium tetrachloroaurate(III) (13682-61-6) + (C4H2NCC6H3(C4H9)2)3(C4H2NCC6H3(O(CH2)2O(CH2)2OC6H4)2C12H6N2)H2 → (C4H2NCC6H3(C4H9)2)3(C4H2NCC6H3(O(CH2)2O(CH2)2OC6H4)2C12H6N2)Au(1+)*PF6(1-) = [C100H104N6O6Au][PF6] (184959-62-4)

Guidance literature:

With sodium acetate; In acetic acid; (argon); refluxing the ligand and the gold salt in HOAc/NaOAc, then ion-exchange with KPF6; chromy.;

DOI:10.1039/cc9960002441

Reference yield: 16.0%

5,10,15-tris[3,5-di(tert-butyl)phenyl]-20-(3,5-dihydroxyphenyl)zinc(II) porphyrin (184959-52-2) + (C100H104N6O6Au)C12H6N2(C6H4O(CH2)2O(CH2)2I)2Cu(2+)*2PF6(1-) = [Cu(C100H104N6O6Au)(C32H30N2O4I2)][PF6]2 → (C4H2NCC6H3(C4H9)2)3(C4H2NCC6H3(O(CH2)2O(CH2)2OC6H4)2C12H6N2)Zn (175090-10-5) + (C4H2NCC6H3(C4H9)2)3(C4H2NCC6H3(O(CH2)2O(CH2)2OC6H4)2C12H6N2)Au(1+)*PF6(1-) = [C100H104N6O6Au][PF6] (184959-62-4) + Cu(1+)*2C100H104N6O6Zn*PF6(1-) = [Cu(C100H104N6O6Zn)2][PF6] + Cu(1+)*Zn(2+)*Au(3+)*2C100H104N6O6(2-)*2PF6(1-) = [Cu(C100H104N6O6Zn)(C100H104N6O6Au)][PF6]2

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; (Ar); 1 day, 60°C; filtn., washing (DMF), solvent removal, CH2Cl2 - aq. KPF6 partitioning, pptn. on DMF and water addn., filtn., dissolving (CH2Cl2), drying (Na2SO4), filtn., concn., chromy. (silica, 1% MeOH in CH2Cl2);

DOI:10.1039/a708756j

upstream raw materials:

potassium hexafluorophosphate

potassium tetrachloroaurate(III)

potassium tetrachloroaurate(III)

5,10,15-tris[3,5-di(tert-butyl)phenyl]-20-(3,5-dihydroxyphenyl)zinc(II) porphyrin

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