C₅₅H₅₂N₄Si₂

Base Information

Chemical Name:C₅₅H₅₂N₄Si₂
CAS No.:1374331-56-2
Molecular Formula:C₅₅H₅₂N₄Si₂
Molecular Weight:825.216
Hs Code.:

C<sub>55</sub>H<sub>52</sub>N<sub>4</sub>Si<sub>2</sub>

Synonyms:C₅₅H₅₂N₄Si₂

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Chemical Property of C₅₅H₅₂N₄Si₂

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Technology Process of C₅₅H₅₂N₄Si₂

There total 3 articles about C₅₅H₅₂N₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1207757-54-7
C₂₃H₁₈Br₂

: 1049806-89-4
4-((4-(trimethylsilyl)phenyl)amino)benzonitrile

: 1374331-56-2
C₅₅H₅₂N₄Si₂

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In toluene; at 95 ℃; for 8h; Inert atmosphere;

Reference yield:

: 319906-45-1
2-bromo-7-iodo-9,9-dimethyl-9H-fluorene

: 1374331-56-2
C₅₅H₅₂N₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -65 °C / Inert atmosphere

1.2: 4 h / 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / -68 °C / Inert atmosphere

2.2: 5 h / 20 °C

3.1: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 8 h / 95 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; tri-tert-butyl phosphine; potassium tert-butylate; sodium t-butanolate; In tetrahydrofuran; hexane; toluene;

Reference yield:

: 6999-03-7
1-bromo-4-(trimethylsilyl)benzene

: 873-74-5
4-Aminobenzonitrile

: 1374331-56-2
C₅₅H₅₂N₄Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 9 h / 105 °C / Inert atmosphere

2: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 8 h / 95 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; In toluene;