7-bromo-2-(4-butylphenyl)phenanthren-4-ol

Base Information

Chemical Name:7-bromo-2-(4-butylphenyl)phenanthren-4-ol
CAS No.:1612866-67-7
Molecular Formula:C₂₄H₂₁BrO
Molecular Weight:405.334
Hs Code.:

Synonyms:7-bromo-2-(4-butylphenyl)phenanthren-4-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-bromo-2-(4-butylphenyl)phenanthren-4-ol

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Technology Process of 7-bromo-2-(4-butylphenyl)phenanthren-4-ol

There total 6 articles about 7-bromo-2-(4-butylphenyl)phenanthren-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100751-63-1
(6-bromo-2-naphthy)methanol

: 1612866-67-7
7-bromo-2-(4-butylphenyl)phenanthren-4-ol

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride; zinc(II) chloride / 1,2-dimethoxyethane / 0 - 20 °C

2.1: water; acetonitrile / Reflux

3.1: acetic acid; sulfuric acid / water / 24 h / 110 °C

4.1: thionyl chloride / 1 h / 90 °C

5.1: 2-Methylpropionic anhydride / 48 h / 190 °C / Inert atmosphere

5.2: 60 - 100 °C

With thionyl chloride; sulfuric acid; 2-Methylpropionic anhydride; acetic acid; zinc(II) chloride; In 1,2-dimethoxyethane; water; acetonitrile;
DOI:10.1002/anie.201310491

Reference yield:

: 33626-98-1
methyl 6-bromo-2-naphthoate

: 1612866-67-7
7-bromo-2-(4-butylphenyl)phenanthren-4-ol

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / tetrahydrofuran; n-heptane / 0 - 20 °C / Inert atmosphere

2.1: thionyl chloride; zinc(II) chloride / 1,2-dimethoxyethane / 0 - 20 °C

3.1: water; acetonitrile / Reflux

4.1: acetic acid; sulfuric acid / water / 24 h / 110 °C

5.1: thionyl chloride / 1 h / 90 °C

6.1: 2-Methylpropionic anhydride / 48 h / 190 °C / Inert atmosphere

6.2: 60 - 100 °C

With thionyl chloride; sulfuric acid; 2-Methylpropionic anhydride; diisobutylaluminium hydride; acetic acid; zinc(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; n-heptane; water; acetonitrile;
DOI:10.1002/anie.201310491

Reference yield:

: 689290-84-4
2-bromo-6-(chloromethyl)naphthalene

: 1612866-67-7
7-bromo-2-(4-butylphenyl)phenanthren-4-ol

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; acetonitrile / Reflux

2.1: acetic acid; sulfuric acid / water / 24 h / 110 °C

3.1: thionyl chloride / 1 h / 90 °C

4.1: 2-Methylpropionic anhydride / 48 h / 190 °C / Inert atmosphere

4.2: 60 - 100 °C

With thionyl chloride; sulfuric acid; 2-Methylpropionic anhydride; acetic acid; In water; acetonitrile;
DOI:10.1002/anie.201310491