cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate

Base Information

Chemical Name:cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate
CAS No.:99572-12-0
Molecular Formula:C₂₄H₃₂O₆S₂
Molecular Weight:484.615
Hs Code.:

Synonyms:cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate

Chemical Property:

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Technology Process of cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate

There total 3 articles about cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 99572-11-9
cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane

: 98-59-9
p-toluenesulfonyl chloride

: 99572-12-0
cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate

Guidance literature:: With pyridine;
DOI:10.1021/ja00263a017

Reference yield:

: 99572-05-1
cis,cis,cis-2,3-dimethyl-1,4-cyclohexanedicarboxylic acid

: 99572-12-0
cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / boron trifluoride etherate / 24 h / Heating

2: 99 percent / lithium aluminum deuteride / diethyl ether / 36 h / Heating

3: 23 percent / pyridine

With pyridine; lithium aluminium deuteride; boron trifluoride diethyl etherate; In diethyl ether;
DOI:10.1021/ja00263a017

Reference yield:

: 99572-06-2
dimethyl cis,cis,cis-2,3-dimethyl-1,4-cyclohexanedicarboxylate

: 99572-12-0
cis,cis,cis-2,3-dimethyl-1,4-bis(dideuteriohydroxymethyl)cyclohexane ditosylate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / lithium aluminum deuteride / diethyl ether / 36 h / Heating

2: 23 percent / pyridine

With pyridine; lithium aluminium deuteride; In diethyl ether;
DOI:10.1021/ja00263a017