Technology Process of N-<4-(2-Amino-ethyl)-phenyl>-diethanolamin
There total 6 articles about N-<4-(2-Amino-ethyl)-phenyl>-diethanolamin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / sat. aq. NaHCO3 / tetrahydrofuran / 0 - 20 °C
2: H2 / 10percent Pd/C / methanol / 2 h / 2068.6 Torr
3: 3-A molecular sieves, NaBH3CN / CHCl3
4: HCl / dioxane
With
hydrogenchloride; 3 A molecular sieve; hydrogen; sodium cyanoborohydride; sodium hydrogencarbonate;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; methanol; chloroform;
DOI:10.1021/jm00101a002
- Guidance literature:
-
Multi-step reaction with 3 steps
1: H2 / 10percent Pd/C / methanol / 2 h / 2068.6 Torr
2: 3-A molecular sieves, NaBH3CN / CHCl3
3: HCl / dioxane
With
hydrogenchloride; 3 A molecular sieve; hydrogen; sodium cyanoborohydride;
palladium on activated charcoal;
In
1,4-dioxane; methanol; chloroform;
DOI:10.1021/jm00101a002
- Guidance literature:
-
Multi-step reaction with 2 steps
1: NaOAc / acetic acid
2: H2, aq. NH3 / Raney-Ni
With
ammonium hydroxide; hydrogen; sodium acetate;
nickel;
In
acetic acid;
DOI:10.1021/jo01067a094
