4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

Base Information

Chemical Name:4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate
CAS No.:1430971-68-8
Molecular Formula:CF₃O₃S*C₆₆H₅₉N₂O₁₇
Molecular Weight:1301.27
Hs Code.:

4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

Synonyms:4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

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Chemical Property of 4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

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Technology Process of 4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

There total 2 articles about 4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1300064-56-5
4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--6--O--triisopropylsilyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

: 1430971-68-8
4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

Guidance literature:: With hydrogenchloride; In dichloromethane; water; at 20 ℃;
DOI:10.1039/c2cc37164b

Reference yield: 10.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1300064-64-5
2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-α-D-glucopyranoside trichloroacetimidate

: 1300064-53-2
C₃₉H₃₇N₂O₉⁽¹⁺⁾

: 1430971-68-8
4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

: 1430971-76-8
4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

: 1430971-91-7
4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--6--O--(2,3,4--tri--O--benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranosyl)--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

Guidance literature:: 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-α-D-glucopyranoside trichloroacetimidate; C₃₉H₃₇N₂O₉⁽¹⁺⁾; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 ℃; for 1h; Molecular sieve;

trimethylsilyl trifluoromethanesulfonate; 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-α-D-glucopyranoside trichloroacetimidate; Further stages;
DOI:10.1039/c2cc37164b

Reference yield: 94.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1300064-64-5
2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-α-D-glucopyranoside trichloroacetimidate

: 1430971-68-8
4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

: 1430971-72-4
4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--6--O--(2,3,4--tri--O--benzoyl--6--O--triisopropylsilyl--β--D--glucopyranosyl)--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate

Guidance literature:: 2,3,4-tri-O-benzoyl-6-O-triisopropylsilyl-α-D-glucopyranoside trichloroacetimidate; 4--(1--methyl--3--methyleneimidazolium)--benzyl 2,3,4--tri--O-benzoyl--6--O--(2,3,4--tri--O--benzoyl--β--D--glucopyranosyl)--β--D--glucopyranoside trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve;

trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -40 - 20 ℃; Molecular sieve;
DOI:10.1039/c2cc37164b