1-(3,5-Bis-phenyl)-2-pentanol

Base Information

Chemical Name:1-(3,5-Bis-phenyl)-2-pentanol
CAS No.:76280-67-6
Molecular Formula:C₁₅H₂₄O₅
Molecular Weight:284.353
Hs Code.:

1-(3,5-Bis<methoxymethoxy>-phenyl)-2-pentanol

Synonyms:1-(3,5-Bis-phenyl)-2-pentanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3,5-Bis-phenyl)-2-pentanol

Chemical Property:

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Technology Process of 1-(3,5-Bis-phenyl)-2-pentanol

There total 6 articles about 1-(3,5-Bis-phenyl)-2-pentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 76280-64-3
2-(3,5-Bis-phenyl)-2-(1-hydroxy-1-butyl)-1,3-dithiane

: 76280-67-6
1-(3,5-Bis-phenyl)-2-pentanol

Guidance literature:: With nickel; sodium carbonate; In ethanol; for 19h; Heating;
DOI:10.1055/s-1980-29193

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 76280-67-6
1-(3,5-Bis-phenyl)-2-pentanol

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / K₂CO₃ / acetonitrile / 1.) ice temp, 1 h

2: 95 percent / LiAlH₄ / diethyl ether / Heating

3: 88 percent / Pyridinium chlorochromate, CH₃COONa / CH₂Cl₂ / 2 h / 24 - 25 °C

4: 71 percent / 1.) MgSO₄, 2.) BF₃ etherate / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) room temp.

5: 98 percent / 1.) Butyllithium / hexane; tetrahydrofuran / 1.5 h / 1.) Dry Ice/acetone bath, 1 h, 2.) Dry Ice/acetone bath, 30 min

6: 82 percent / Raney Ni, Na₂CO₃ / ethanol / 19 h / Heating

With lithium aluminium tetrahydride; n-butyllithium; boron trifluoride diethyl etherate; sodium acetate; nickel; sodium carbonate; magnesium sulfate; potassium carbonate; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; acetonitrile;
DOI:10.1055/s-1980-29193

Reference yield:

: 76280-60-9
[3,5-bis(methoxymethoxy)phenyl]methanol

: 76280-67-6
1-(3,5-Bis-phenyl)-2-pentanol

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / Pyridinium chlorochromate, CH₃COONa / CH₂Cl₂ / 2 h / 24 - 25 °C

2: 71 percent / 1.) MgSO₄, 2.) BF₃ etherate / tetrahydrofuran / 1.) 0 deg C, 1 h, 2.) room temp.

3: 98 percent / 1.) Butyllithium / hexane; tetrahydrofuran / 1.5 h / 1.) Dry Ice/acetone bath, 1 h, 2.) Dry Ice/acetone bath, 30 min

4: 82 percent / Raney Ni, Na₂CO₃ / ethanol / 19 h / Heating

With n-butyllithium; boron trifluoride diethyl etherate; sodium acetate; nickel; sodium carbonate; magnesium sulfate; pyridinium chlorochromate; In tetrahydrofuran; ethanol; hexane; dichloromethane;
DOI:10.1055/s-1980-29193