3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide

Base Information

Chemical Name:3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide
CAS No.:302554-72-9
Molecular Formula:C₁₈H₁₅N₅O₂S
Molecular Weight:365.415
Hs Code.:

Synonyms:3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide

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Technology Process of 3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide

There total 7 articles about 3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 302554-40-1
3-amino-4-(p-methoxyphenyl)cyclopenta[e]thieno[2,3-b]pyridine-2-carbohydrazide

: 302554-72-9
3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide

Guidance literature:: With sodium nitrite; In acetic acid; at 20 ℃; for 0.0833333h;

Reference yield:

: 68029-57-2
2-cyano-3-(4-methoxyphenyl)thioacrylamide

: 302554-72-9
3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide

Guidance literature:: Multi-step reaction with 5 steps

1.1: piperidine / ethanol / 3 h / Heating

1.2: Et₃N / ethanol / 2 h / Heating

2.1: NaOEt / ethanol / 1 h / Heating

3.1: 80 percent / CH₃CO₂Na*3H₂O / ethanol / 2 h / Heating

4.1: 75 percent / N₂H₄*H₂O / 2 h / Heating

5.1: 82 percent / NaNO₂ / acetic acid / 0.08 h / 20 °C

With piperidine; sodium ethanolate; sodium acetate; hydrazine hydrate; sodium nitrite; In ethanol; acetic acid;

Reference yield:

: 120-92-3
cyclopentanone

: 302554-72-9
3-amino-4-(p-methoxyphenyl)-cyclopenta[e]thieno[2,3-b]pyridine-2-carbonylazide

Guidance literature:: Multi-step reaction with 5 steps

1.1: piperidine / ethanol / 3 h / Heating

1.2: Et₃N / ethanol / 2 h / Heating

2.1: NaOEt / ethanol / 1 h / Heating

3.1: 80 percent / CH₃CO₂Na*3H₂O / ethanol / 2 h / Heating

4.1: 75 percent / N₂H₄*H₂O / 2 h / Heating

5.1: 82 percent / NaNO₂ / acetic acid / 0.08 h / 20 °C

With piperidine; sodium ethanolate; sodium acetate; hydrazine hydrate; sodium nitrite; In ethanol; acetic acid;