N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine

Base Information

• Chemical Name: N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine
• CAS No.: 1096706-37-4
• Molecular Formula: C₁₅H₁₇F₂N₇
• Molecular Weight: 333.344

Synonyms:N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine

Chemical Property of N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine

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Technology Process of N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine

There total 1 articles about N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.8%

1,2,4-Triazole (288-88-0) + 2-bromo-N-(2-bromoethyl)-N-(2,4-difluorobenzyl)ethanamine (1096706-55-6) → N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine (1096706-37-4)

Guidance literature:

1,2,4-Triazole; With potassium carbonate; In acetonitrile; at 60 ℃; for 1h;

2-bromo-N-(2-bromoethyl)-N-(2,4-difluorobenzyl)ethanamine; In acetonitrile; at 20 - 60 ℃;

DOI:10.1016/j.ejmech.2010.06.012

Reference yield: 72.2%

N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine (1096706-37-4) → N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine trihydrochloride

Guidance literature:

With hydrogenchloride; In diethyl ether; chloroform;

DOI:10.1016/j.ejmech.2010.06.012

Reference yield: 65.1%

N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine (1096706-37-4) → N-(2-(1H-1,2,4-triazol-1-yl)ethyl)-N-(2,4-difluorobenzyl)-2-(1H-1,2,4-triazol-1-yl)ethanamine trinitrate

Guidance literature:

With nitric acid; In diethyl ether; chloroform;

DOI:10.1016/j.ejmech.2010.06.012

upstream raw materials:

1,2,4-Triazole

2-bromo-N-(2-bromoethyl)-N-(2,4-difluorobenzyl)ethanamine

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