C₂₉H₂₈O₄S₂

Base Information

Chemical Name:C₂₉H₂₈O₄S₂
CAS No.:136202-26-1
Molecular Formula:C₂₉H₂₈O₄S₂
Molecular Weight:504.671
Hs Code.:

C<sub>29</sub>H<sub>28</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:C₂₉H₂₈O₄S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₈O₄S₂

Chemical Property:

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Technology Process of C₂₉H₂₈O₄S₂

There total 5 articles about C₂₉H₂₈O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60526-40-1
7-Spirocyclopropanbicyclo[2.2.1]hept-5-en-2,3-dion

: 136202-26-1
C₂₉H₂₈O₄S₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) THF, overnight, 2.) THF, a) RT, 2 h, b) 45 deg C, 3 d

2: 1.) KH / 1.) DMF, THF, -45 deg C, 30 min, 2.) DMF, THF, RT, overnight

3: 100 percent / tetrahydrofuran / 120 h / 8274370 Torr

4: 1.) CH₂Cl₂, Et₂O, 0 deg C, overnight, 2.) CH₂Cl₂, acetone, irradiation, 45 min

With n-butyllithium; potassium hydride; In tetrahydrofuran;
DOI:10.1021/ja00103a004

Reference yield:

: 166805-27-2
C₁₂H₁₂

: 136202-26-1
C₂₉H₂₈O₄S₂

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) KH / 1.) DMF, THF, -45 deg C, 30 min, 2.) DMF, THF, RT, overnight

2: 100 percent / tetrahydrofuran / 120 h / 8274370 Torr

3: 1.) CH₂Cl₂, Et₂O, 0 deg C, overnight, 2.) CH₂Cl₂, acetone, irradiation, 45 min

With potassium hydride; In tetrahydrofuran;
DOI:10.1021/ja00103a004

Reference yield:

: 166805-28-3
C₁₄H₁₄

: 136202-26-1
C₂₉H₂₈O₄S₂

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / tetrahydrofuran / 120 h / 8274370 Torr

2: 1.) CH₂Cl₂, Et₂O, 0 deg C, overnight, 2.) CH₂Cl₂, acetone, irradiation, 45 min

In tetrahydrofuran;
DOI:10.1021/ja00103a004