ETHYL 2-ACETYLOXY-A-(1-HYDROXYETHYLIDENE)-B-OXOBENZENE PROPANOATE

Base Information

Chemical Name:ETHYL 2-ACETYLOXY-A-(1-HYDROXYETHYLIDENE)-B-OXOBENZENE PROPANOATE
CAS No.:92397-13-2
Molecular Formula:C₁₅H₁₆O₆
Molecular Weight:292.288
Hs Code.:
Mol file:92397-13-2.mol

Synonyms:ETHYL 2-ACETYLOXY-A-(1-HYDROXYETHYLIDENE)-B-OXOBENZENE PROPANOATE;Ethyl 2-acetyloxy-(1-hydroxyethylidene)-oxobenzene propanoate;Ethyl-(2-acetoxybenzoyl)acetoacetate

Suppliers and Price of ETHYL 2-ACETYLOXY-A-(1-HYDROXYETHYLIDENE)-B-OXOBENZENE PROPANOATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
ETHYL-2-ACETYLOXY-ALPHA-(1-HYDROXYETHYLIDENE)-BETA-OXOBENZENE PROPANOATE 95.00%
5MG
$ 501.90

Total 3 raw suppliers

Chemical Property of ETHYL 2-ACETYLOXY-A-(1-HYDROXYETHYLIDENE)-B-OXOBENZENE PROPANOATE

Chemical Property:

PSA：89.90000
LogP:2.18970

Purity/Quality:: ETHYL-2-ACETYLOXY-ALPHA-(1-HYDROXYETHYLIDENE)-BETA-OXOBENZENE PROPANOATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ETHYL 2-ACETYLOXY-A-(1-HYDROXYETHYLIDENE)-B-OXOBENZENE PROPANOATE

There total 1 articles about ETHYL 2-ACETYLOXY-A-(1-HYDROXYETHYLIDENE)-B-OXOBENZENE PROPANOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 141-97-9
ethyl acetoacetate

: 5538-51-2
O-acetylsalicyloyl chloride

: 92397-13-2
(E)-2-(2-Acetoxy-benzoyl)-3-hydroxy-but-2-enoic acid ethyl ester

Guidance literature:: With magnesium ethylate; Multistep reaction; 1) toluene, reflux, 2 h, 2) CH₃CN, room temperature, 3 h;
DOI:10.1021/jo00197a018

Reference yield:

: 92397-13-2
(E)-2-(2-Acetoxy-benzoyl)-3-hydroxy-but-2-enoic acid ethyl ester

: 92397-18-7
ethyl 5-(2-hydroxyphenyl)-3-methylisooxazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride, ethanol / 1 h / Heating

2: 48 percent / NH₂OH*HCl, pyridine / 1 h / Heating

With pyridine; ethanol; hydroxylamine hydrochloride; acetyl chloride;
DOI:10.1021/jo00197a018