3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate

Base Information

Chemical Name:3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate
CAS No.:1344121-73-8
Molecular Formula:C₄₀H₆₂N₃O₉P
Molecular Weight:759.921
Hs Code.:

Synonyms:3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate

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Chemical Property of 3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate

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Technology Process of 3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate

There total 3 articles about 3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 23377-40-4
3-hexadecyloxy-1-propanol

: 1414873-33-8
C₆H₁₅N*C₂₁H₂₄N₃O₈P

: 1344121-73-8
3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate

Guidance literature:: With 2,4,6-triisopropylphenylsulfonyl chloride; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm2009343

Reference yield:

: 1414873-30-5
C₂₂H₂₆N₃O₈P

: 1344121-73-8
3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; water / 60 °C / Inert atmosphere

2: Dowex 50 / ethanol / 0.17 h / Inert atmosphere

3: 2,4,6-triisopropylphenylsulfonyl chloride / dichloromethane / 20 °C / Inert atmosphere

With pyridine; 2,4,6-triisopropylphenylsulfonyl chloride; water; In ethanol; dichloromethane;
DOI:10.1021/jm2009343

Reference yield:

: 1344121-63-6
4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate

: 1344121-73-8
3-(hexadecyloxy)propyl 4-N-benzoyl-2',3'-isopropylidenecytidin-5'-yl vinylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: Dowex 50 / ethanol / 0.17 h / Inert atmosphere

2: 2,4,6-triisopropylphenylsulfonyl chloride / dichloromethane / 20 °C / Inert atmosphere

With 2,4,6-triisopropylphenylsulfonyl chloride; In ethanol; dichloromethane;
DOI:10.1021/jm2009343