Cycloheptanesulfonamide, 2-oxo- (9CI)

Base Information

Chemical Name:Cycloheptanesulfonamide, 2-oxo- (9CI)
CAS No.:96855-97-9
Molecular Formula:C7H13 N O3 S
Molecular Weight:191.24802
Hs Code.:
Mol file:96855-97-9.mol

Synonyms:Cycloheptanesulfonamide, 2-oxo- (9CI)

Suppliers and Price of Cycloheptanesulfonamide, 2-oxo- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cycloheptanesulfonamide, 2-oxo- (9CI)

Chemical Property:

Melting Point:76 - 78 °C (propan-2-ol)
PSA：85.61000
LogP:1.95780

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Cycloheptanesulfonamide, 2-oxo- (9CI)

There total 3 articles about Cycloheptanesulfonamide, 2-oxo- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1020841-99-9
2-oxo-cycloheptanesulfonyl chloride

: 96855-97-9
2-oxocycloheptylsulfonamide

Guidance literature:: With ammonia; In dichloromethane; Cooling;
DOI:10.1021/jf0403944

Reference yield:

: potassium 2-oxocycloheptylsulfonate

: 96855-97-9
2-oxocycloheptylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 1.5 h / Heating

2: NH₃ (gas) / CH₂Cl₂ / Cooling

With oxalyl dichloride; ammonia; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/jf0403944

Reference yield:

: 96855-97-9
2-oxocycloheptylsulfonamide

Guidance literature:: With sulphamoyl chloride; silica gel; triethylamine; Yield given. Multistep reaction; 1.) THF, -40 deg C -> 20 deg C, 2 h, 2.) CH2Cl2;
DOI:10.1055/s-1985-31109