benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate

Base Information

Chemical Name:benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate
CAS No.:867262-96-2
Molecular Formula:C₂₆H₃₄N₂O₅
Molecular Weight:454.566
Hs Code.:

Synonyms:benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate

Suppliers and Price of benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate

There total 8 articles about benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₂₆N₂O₄

: 100-51-6,185532-71-2
benzyl alcohol

: 867262-96-2
benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate

Guidance literature:: In toluene; at 20 - 100 ℃; for 8.5h;

Reference yield:

: 850887-58-0
Methyl cis-4-[(diphenylmethyl)amino]-1-(3-methoxyphenyl)-cyclohexanecarboxylate

: 867262-96-2
benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 3 h / 20 °C / 2250.23 Torr

2.1: potassium hydroxide; water / dimethyl sulfoxide / 1.5 h / 20 - 50 °C

2.2: 20 °C / pH 4

3.1: diphenyl phosphoryl azide; triethylamine / toluene / 8 h / 80 °C

4.1: toluene / 8.5 h / 20 - 100 °C

With potassium hydroxide; diphenyl phosphoryl azide; water; hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dimethyl sulfoxide; toluene;

Reference yield:

: 867262-67-7
dimethyl 1-(3-methoxyphenyl)-4-oxocyclohexane-1,3-dicarboxylate

: 867262-96-2
benzyl tert-butyl [cis-1-(3-methoxyphenyl)cyclohexan-1,4-diyl]biscarbamate

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide; water / 1,4-dioxane / 5 h / Heating / reflux

1.2: 4 h / 60 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 - 35 °C

3.1: sodium cyanoborohydride; acetic acid / methanol / 72 h / 0 - 20 °C

4.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 3 h / 20 °C / 2250.23 Torr

5.1: potassium hydroxide; water / dimethyl sulfoxide / 1.5 h / 20 - 50 °C

5.2: 20 °C / pH 4

6.1: diphenyl phosphoryl azide; triethylamine / toluene / 8 h / 80 °C

7.1: toluene / 8.5 h / 20 - 100 °C

With potassium hydroxide; diphenyl phosphoryl azide; water; hydrogen; sodium cyanoborohydride; potassium carbonate; acetic acid; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;