(E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane

Base Information

Chemical Name:(E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane
CAS No.:11997-33-4
Molecular Formula:C₂₂H₃₀OSi
Molecular Weight:338.565
Hs Code.:

Synonyms:(E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane

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Chemical Property of (E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane

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Technology Process of (E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane

There total 2 articles about (E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: tert-butyl({[(2RS,3RS)-2,3-dichlorohexyl]oxy})diphenylsilane

: 11997-33-4
(E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium iodide; at 160 ℃; for 2h;
DOI:10.1021/jo802093d

Reference yield: 95.0%

: 928-95-0
(E)-2-Hexen-1-ol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 11997-33-4
(E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane

Guidance literature:: With 1H-imidazole; triethylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jacs.7b12316

Reference yield: 71.0%

: 11997-33-4
(E)-tert-butyl(hex-2-en-1-yloxy)diphenylsilane

: tert-butyl({[(2RS,3RS)-2,3-dichlorohexyl]oxy})diphenylsilane

Guidance literature:: With 2,6-lutidine N-oxide; chloro-trimethyl-silane; diphenyl diselenide; N-benzyl-N,N,N-triethylammonium chloride; 1-fluoro-pyridinium tetrafluoroborate; In acetonitrile; at 20 ℃; for 7h; stereospecific reaction; Sealed tube; Inert atmosphere;
DOI:10.1038/nchem.2141