3-acetyl-4-methanesulfonylaminobenzoic acid

Base Information

Chemical Name:3-acetyl-4-methanesulfonylaminobenzoic acid
CAS No.:960324-79-2
Molecular Formula:C₁₀H₁₁NO₅S
Molecular Weight:257.267
Hs Code.:

Synonyms:3-acetyl-4-methanesulfonylaminobenzoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-acetyl-4-methanesulfonylaminobenzoic acid

Chemical Property:

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Technology Process of 3-acetyl-4-methanesulfonylaminobenzoic acid

There total 3 articles about 3-acetyl-4-methanesulfonylaminobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₃NO₅S

: 960324-79-2
3-acetyl-4-methanesulfonylaminobenzoic acid

Guidance literature:: With methanol; lithium hydroxide; water; In tetrahydrofuran; at 110 ℃; for 0.5h; Microwave irradiation;

Reference yield:

: 111714-47-7
3-acetyl-4-aminobenzoic acid methyl ester

: 960324-79-2
3-acetyl-4-methanesulfonylaminobenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dmap / dichloromethane / 1 - 16 h

2: methanol; lithium hydroxide; water / tetrahydrofuran / 0.5 h / 110 °C / Microwave irradiation

With pyridine; methanol; lithium hydroxide; water; dmap; In tetrahydrofuran; dichloromethane;

Reference yield:

: 177913-49-4
5-acetyl-4-amino-1-hydroxycyclohexa-2,4-dienecarboxylic acid methyl ester

: 960324-79-2
3-acetyl-4-methanesulfonylaminobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / benzene / 0.5 h / Heating / reflux

2: pyridine / dmap / dichloromethane / 1 - 16 h

3: methanol; lithium hydroxide; water / tetrahydrofuran / 0.5 h / 110 °C / Microwave irradiation

With pyridine; methanol; lithium hydroxide; boron trifluoride diethyl etherate; water; dmap; In tetrahydrofuran; dichloromethane; benzene;