phenylmethyl 2-<<carbonyl>amino>-5-hexenoate

Base Information

Chemical Name:phenylmethyl 2-<<carbonyl>amino>-5-hexenoate
CAS No.:222739-31-3
Molecular Formula:C₂₁H₂₃NO₅
Molecular Weight:369.417
Hs Code.:

phenylmethyl 2-<<<tetrahydro-5-oxo-2-(2-propynyl)-2-furanyl>carbonyl>amino>-5-hexenoate

Synonyms:phenylmethyl 2-<<carbonyl>amino>-5-hexenoate

Suppliers and Price of phenylmethyl 2-<<carbonyl>amino>-5-hexenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenylmethyl 2-<<carbonyl>amino>-5-hexenoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenylmethyl 2-<<carbonyl>amino>-5-hexenoate

There total 6 articles about phenylmethyl 2-<<carbonyl>amino>-5-hexenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 179815-17-9
tetrahydro-5-oxo-2-<2-(propynyl)>-2-furancarboxylic acid

: 206867-88-1
phenylmethyl 2-amino-5-hexenoate

: 222739-31-3
phenylmethyl 2-<<carbonyl>amino>-5-hexenoate

Guidance literature:: With 1-hydroxybenzotriazol-hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(98)00384-0

Reference yield: 46.0%

: 179815-17-9
tetrahydro-5-oxo-2-<2-(propynyl)>-2-furancarboxylic acid

: 206867-88-1
phenylmethyl 2-amino-5-hexenoate

: 222739-31-3
phenylmethyl 2-<<carbonyl>amino>-5-hexenoate

: phenylmethyl (2S)-2-<<carbonyl>amino>-5-hexenoate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1021/jo9822941

Reference yield:

: 193223-82-4
phenylmethyl 2-<<(1,1-dimethylethoxy)carbonyl>amino>-5-hexenoate

: 222739-31-3
phenylmethyl 2-<<carbonyl>amino>-5-hexenoate

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂ / 0.5 h / 0 - 20 °C

2: 1-hydroxybenzotriazole, 1-(3-(dimethylamino)propyl)-3-ethylcarbodiimide hydrochloride / CH₂Cl₂; dimethylformamide / 12 h / Ambient temperature

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo9822941