N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide

Base Information

• Chemical Name: N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide
• CAS No.: 606969-34-0
• Molecular Formula: C₁₆H₂₀N₆O₄S₂
• Molecular Weight: 424.505

Synonyms:N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide

Chemical Property of N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide

Chemical Property:

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Technology Process of N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide

There total 5 articles about N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.4%

N-imidazo[1,2-d][1,2,4]thiadiazol-3-ylhexane-1,6-diamine (606969-04-4) + 2-Nitrobenzenesulfonyl chloride (1694-92-4) → N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide (606969-34-0)

Guidance literature:

With potassium carbonate; In acetone;

DOI:10.1021/jm049221w

Reference yield: 70.4%

→ N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide (606969-34-0)

Guidance literature:

Reference yield: 58.0%

3-[(4-methylphenyl)sulfonyl]imidazo[1,2-d][1,2,4]thiadiazole (606969-03-3) + N-(6-aminohexyl)-2'-nitrobenzenesulfonamide (655246-57-4) → N-[6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl]-2-nitrobenzenesulfonamide (606969-34-0)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide;

DOI:10.1021/jo0507486

upstream raw materials:

N-imidazo[1,2-d][1,2,4]thiadiazol-3-ylhexane-1,6-diamine

2-Nitrobenzenesulfonyl chloride

3-[(4-methylphenyl)sulfonyl]imidazo[1,2-d][1,2,4]thiadiazole

N-(6-aminohexyl)-2'-nitrobenzenesulfonamide

Downstream raw materials:

tert-butyl [6-(imidazo[1,2-d][1,2,4]thiadiazol-3-ylamino)hexyl][(2-nitrophenyl)sulfonyl]carbamate

t-butyl [6-(imidazo[1,2-d][1,2,4]thiadiazol-3-yl(methyl)amino)hexyl][(2-nitrophenyl)sulfonyl]carbamate

methyl N-(6-{(tert-butoxycarbonyl)[(2-nitrophenyl)sulfonyl]-amino}hexyl)-N-imidazo[1,2-d][1,2,4]thiadiazol-3-ylglycinate

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