endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride

Base Information

Chemical Name:endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride
CAS No.:123259-36-9
Molecular Formula:C₁₅H₁₉N₃O₄*ClH
Molecular Weight:341.794
Hs Code.:

Synonyms:endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride

Chemical Property:

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Technology Process of endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride

There total 2 articles about endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123259-23-4
endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl chloroformate hydrochloride

: 88-74-4
2-nitro-aniline

: 123259-36-9
endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride

Guidance literature:: In pyridine; at 80 ℃; for 4h;
DOI:10.1021/jm00170a009

Reference yield:

: 2292-08-2
tropine hydrochloride

: 123259-36-9
endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / acetonitrile / 1.) O deg C, 30 min, 2.) RT, 24 h

2: 6.5 g / pyridine / 4 h / 80 °C

In pyridine; acetonitrile;
DOI:10.1021/jm00170a009

Reference yield:

: 123259-36-9
endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-nitrophenyl)carbamate hydrochloride

: 123259-35-8
endo-8-methyl-8-azabicyclo<3.2.1>oct-3-yl N-(2-aminophenyl)carbamate

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; water; under 760 Torr; Ambient temperature;
DOI:10.1021/jm00170a009