[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl]⁽²⁺⁾*2BF₄^(1-)=[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl](BF₄)2

Base Information

• Chemical Name: [(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl]⁽²⁺⁾*2BF₄^(1-)=[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl](BF₄)2
• CAS No.: 81141-65-3
• Molecular Formula: 2BF₄*C₄₁H₅₂ClCu₂N₂O₃P₂RhS₄
• Molecular Weight: 1250.15

Synonyms:[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl]⁽²⁺⁾*2BF₄^(1-)=[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl](BF₄)2

Chemical Property of [(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl]⁽²⁺⁾*2BF₄^(1-)=[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl](BF₄)2

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Technology Process of [(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl]⁽²⁺⁾*2BF₄^(1-)=[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl](BF₄)2

There total 1 articles about [(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl]⁽²⁺⁾*2BF₄^(1-)=[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl](BF₄)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrakis(acetonitrile)copper(I)tetrafluoroborate + [Rh(CO)Cl(O(CH2CH2SCH2CH2)2NP(C6H5)2)2] (81141-61-9) → [(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](2+)*2BF4(1-)=[(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](BF4)2 (81141-65-3)

Guidance literature:

In acetonitrile; MeCN soln. contg. 2 equiv of Cu(MeCN)4BF4 added to soln. of Rh complex under Ar; ppt. isolated on addn. of methanol; elem. anal.;

DOI:10.1021/ja00373a051

Reference yield:

[(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](2+)*2BF4(1-)=[(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](BF4)2 (81141-65-3) → [CO(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](2+)*2BF4(1-)=[CO(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](BF4)2 (81157-70-2)

Guidance literature:

With carbon monoxide; In acetonitrile; Rh complex reacts with CO in MeCN soln. at reflux; elem. anal.;

DOI:10.1021/ja00373a051

Reference yield:

[(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](2+)*2BF4(1-)=[(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](BF4)2 (81141-65-3) → [CO(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](2+)*2BF4(1-)=[CO(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2Rh(CO)Cl](BF4)2 (81157-70-2) + [(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2RhCl](2+)*2BF4(1-)=[(Cu(O(CH2CH2SCH2CH2)2NP(C6H5)2))2RhCl](BF4)2 (81157-65-5)

Guidance literature:

In acetonitrile; reflux in MeCN soln. under Ar for ca. 1 h; not isolated; detected by NMR;

DOI:10.1021/ja00373a051

upstream raw materials:

[Rh(CO)Cl(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2)2]

Downstream raw materials:

[CO(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl]⁽²⁺⁾*2BF₄^(1-)=[CO(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2Rh(CO)Cl](BF₄)2

[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2RhCl]⁽²⁺⁾*2BF₄^(1-)=[(Cu(O(CH₂CH₂SCH₂CH₂)2NP(C₆H₅)2))2RhCl](BF₄)2

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