(3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine

Base Information

• Chemical Name: (3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine
• CAS No.: 524012-99-5
• Molecular Formula: C₂₄H₂₆FNO₆
• Molecular Weight: 443.472

Synonyms:(3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine

Chemical Property of (3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine

Chemical Property:

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Technology Process of (3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine

There total 5 articles about (3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

glutaric anhydride, (108-55-4) + (+/-)-trans-4-(4'-fluorophenyl)-3-hydroxymethyl-N-phenyloxycarbonylpiperidine → (3S,4R)-(-)-4-(4'-fluorophenyl)-3-hydroxymethyl-N-phenyloxycarbonylpiperidine (392328-30-2) + (3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine (524012-99-5)

Guidance literature:

With lipase CAL-B; In tert-butyl methyl ether; at 30 ℃;

Reference yield:

glutaric anhydride, (108-55-4) + (+/-)-trans-4-(4'-fluorophenyl)-3-hydroxymethyl-N-phenyloxycarbonylpiperidine → (3R,4S)-(+)-4-(4'-fluorophenyl)-3-hydroxymethyl-N-phenyloxycarbonylpiperidine (392328-31-3) + (3S,4R)-(-)-4-(4'-fluorophenyl)-3-hydroxymethyl-N-phenyloxycarbonylpiperidine (392328-30-2) + (3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine (524012-99-5)

Guidance literature:

With lipase CAL-B; In toluene; at 15 - 30 ℃;

Reference yield:

glutaric anhydride, (108-55-4) + (+/-)-trans-4-(4'-fluorophenyl)-3-hydroxymethyl-N-phenyloxycarbonylpiperidine → (3R,4S)-(+)-4-(4'-fluorophenyl)-3-hydroxymethyl-N-phenyloxycarbonylpiperidine (392328-31-3) + (3S,4R)-(-)-4-(4'-fluorophenyl)-3-hydroxymethyl-N-phenyloxycarbonylpiperidine (392328-30-2) + (3R,4S)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine (524012-99-5) + (3S,4R)-3-[(3-carboxybutanoyl)oxymethyl]-4-(4'-fluorophenyl)-N-phenyloxycarbonylpiperidine

Guidance literature:

With lipase CAL-A; In toluene; at 30 ℃;

upstream raw materials:

glutaric anhydride,

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