C₃₀H₂₉N₃O₆

Base Information

Chemical Name:C₃₀H₂₉N₃O₆
CAS No.:321172-91-2
Molecular Formula:C₃₀H₂₉N₃O₆
Molecular Weight:527.577
Hs Code.:

C<sub>30</sub>H<sub>29</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C₃₀H₂₉N₃O₆

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Chemical Property of C₃₀H₂₉N₃O₆

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Technology Process of C₃₀H₂₉N₃O₆

There total 21 articles about C₃₀H₂₉N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 321172-62-7
C₃₄H₃₇N₃O₆

: 321172-91-2
C₃₀H₂₉N₃O₆

Guidance literature:: With formic acid;

Reference yield:

: 321172-31-0
(1R,2R,3S,4R,7R)-3-Chloro-7-hydroxy-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid methyl ester

: 321172-91-2
C₃₀H₂₉N₃O₆

Guidance literature:: Multi-step reaction with 19 steps

1: 100 percent / tBuOOH; VO(acac)2 / benzene

2: 97 percent / 2,6-lutidine / CH₂Cl₂

3: 98 percent / tBuOK / benzene

4: methylaluminum bis(2,6-di-tert-butyl-4-methylphenoxide) / toluene / -20 °C

5: piperidine / methanol

6: 87 percent / TBAF / tetrahydrofuran

7: CrO₃; H₂SO₄ / acetone

8: toluene; acetonitrile / 90 °C

9: nBuLi / tetrahydrofuran / 65 °C

10: tBuOK

11: 75 percent / nBu₃SnH; AIBN / benzene / Heating

12: 100 percent / methanol

13: 94 percent / pyridine; DMAP / CH₂Cl₂

14: 94 percent / LiBH₄; LiBEt₃H / tetrahydrofuran

15: pyrrolidine / [Pd(PPh₃)4] / tetrahydrofuran

16: DIEA / acetonitrile / 60 °C

17: 62 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

18: 92 percent / pyridine; DMAP / CH₂Cl₂

19: 96 percent / HCO₂H

With pyrrolidine; piperidine; pyridine; 2,6-dimethylpyridine; chromium(VI) oxide; tert.-butylhydroperoxide; dmap; lithium borohydride; n-butyllithium; formic acid; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); sulfuric acid; potassium tert-butylate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; potassium hexamethylsilazane; bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum; lithium triethylborohydride; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; acetonitrile; benzene; 7: Jones' oxidation / 9: Horner-Emmons reaction / 12: Michael addition / 17: Michael addition;

Reference yield:

: 321172-27-4
(1R,2R,3R,4R,7R)-3-Chloro-7-dimethylsilanyl-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid methyl ester

: 321172-91-2
C₃₀H₂₉N₃O₆

Guidance literature:: Multi-step reaction with 20 steps

1: 53 percent / aq. H₂O₂; KF; KHCO₃ / tetrahydrofuran; methanol

2: 100 percent / tBuOOH; VO(acac)2 / benzene

3: 97 percent / 2,6-lutidine / CH₂Cl₂

4: 98 percent / tBuOK / benzene

5: methylaluminum bis(2,6-di-tert-butyl-4-methylphenoxide) / toluene / -20 °C

6: piperidine / methanol

7: 87 percent / TBAF / tetrahydrofuran

8: CrO₃; H₂SO₄ / acetone

9: toluene; acetonitrile / 90 °C

10: nBuLi / tetrahydrofuran / 65 °C

11: tBuOK

12: 75 percent / nBu₃SnH; AIBN / benzene / Heating

13: 100 percent / methanol

14: 94 percent / pyridine; DMAP / CH₂Cl₂

15: 94 percent / LiBH₄; LiBEt₃H / tetrahydrofuran

16: pyrrolidine / [Pd(PPh₃)4] / tetrahydrofuran

17: DIEA / acetonitrile / 60 °C

18: 62 percent / KHMDS / tetrahydrofuran / -78 - 0 °C

19: 92 percent / pyridine; DMAP / CH₂Cl₂

20: 96 percent / HCO₂H

With pyrrolidine; piperidine; pyridine; 2,6-dimethylpyridine; chromium(VI) oxide; tert.-butylhydroperoxide; dmap; potassium fluoride; lithium borohydride; n-butyllithium; formic acid; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); sulfuric acid; potassium tert-butylate; tetrabutyl ammonium fluoride; dihydrogen peroxide; tri-n-butyl-tin hydride; potassium hexamethylsilazane; bis(2,6-di-tert-butyl-4-methylphenoxide)methylaluminum; lithium triethylborohydride; potassium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; acetonitrile; benzene; 8: Jones' oxidation / 10: Horner-Emmons reaction / 13: Michael addition / 18: Michael addition;