pinanediol 4-azido-1-phenylbutylboronate

Base Information

• Chemical Name: pinanediol 4-azido-1-phenylbutylboronate
• CAS No.: 445433-35-2
• Molecular Formula: C₂₀H₂₈BN₃O₂
• Molecular Weight: 353.272

Synonyms:pinanediol 4-azido-1-phenylbutylboronate

Chemical Property of pinanediol 4-azido-1-phenylbutylboronate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

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Technology Process of pinanediol 4-azido-1-phenylbutylboronate

There total 1 articles about pinanediol 4-azido-1-phenylbutylboronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

pinanediol 4-azido-1-chlorobutylboronate + phenylmagnesium bromide → pinanediol 4-azido-1-phenylbutylboronate (445433-35-2)

Guidance literature:

In tetrahydrofuran; at 20 - 25 ℃; for 24h;

DOI:10.1021/ol025973d

Reference yield: 73.0%

pinanediol 4-azido-1-phenylbutylboronate (445433-35-2) → potassium [(1R)-4-azido-1-phenylbutyl]-trifluoroborate

Guidance literature:

With potassium hydrogen difluoride; In methanol; water; at 22 ℃;

DOI:10.1021/ol025973d

Reference yield:

pinanediol 4-azido-1-phenylbutylboronate (445433-35-2) → (2S)-2-phenylpyrrolidine-(S)-MTPA-amide

Guidance literature:

Multi-step reaction with 3 steps

1.1: 73 percent / potassium hydrogen fluoride / methanol; H₂O / 22 °C

2.1: tetrachlorosilane / toluene; acetonitrile / 10 h / 22 °C

2.2: 77 percent / water

3.1: CH₂Cl₂ / 5 h

With tetrachlorosilane; potassium hydrogen difluoride; In methanol; dichloromethane; water; toluene; acetonitrile;

DOI:10.1021/ol025973d

Downstream raw materials:

(R)-2-phenylpyrrolidine

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