7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine

Base Information

Chemical Name:7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine
CAS No.:98704-52-0
Molecular Formula:C₃₃H₃₉NO₅
Molecular Weight:529.676
Hs Code.:

Synonyms:7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine

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Chemical Property of 7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine

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Technology Process of 7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine

There total 4 articles about 7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₁H₁₃BrMgO

: 98704-52-0
7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 6 h / Heating

2: 1.) ethyl azodicarboxylate, 2.) NH₄Cl / 1.) benzene, reflux, 5 h, 2.) water, ethanol, heting, 7 h

With ethyl azodicarboxylate; ammonium chloride; In tetrahydrofuran;
DOI:10.1021/jm00150a032

Reference yield:

: C₁₁H₁₃IMgO

: 98704-52-0
7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 24 h / Heating

2: 1.) ethyl azodicarboxylate, 2.) NH₄Cl / 1.) benzene, reflux, 5 h, 2.) water, ethanol, heting, 7 h

With ethyl azodicarboxylate; ammonium chloride; In diethyl ether;
DOI:10.1021/jm00150a032

Reference yield:

: 98719-88-1
7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine fumarate

: 98704-52-0
7α-<(1R)-1-hydroxy-1-methyl-3-<4-(allyloxy)phenyl>propyl>-6,14-endo-ethenotetrahydronorthebaine

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Na₂CO₃ / acetone; H₂O / 1 h / Heating

2: 1.) ethyl azodicarboxylate, 2.) NH₄Cl / 1.) benzene, reflux, 5 h, 2.) water, ethanol, heting, 7 h

With ethyl azodicarboxylate; sodium carbonate; ammonium chloride; In water; acetone;
DOI:10.1021/jm00150a032