Technology Process of C24H17N5O
There total 9 articles about C24H17N5O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 4-acetamidobenzenesulfonyl azide; triethylamine / dichloromethane / 0 - 20 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C
2.2: 0 °C
3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.17 h / 0 °C
3.2: 1.5 h / 0 - 20 °C
4.1: water; potassium hydroxide / tetrahydrofuran; methanol / 2 h / 70 °C
5.1: triethylamine; HATU / N,N-dimethyl-formamide / 20 °C
6.1: acetic acid / 3 h / 130 °C
7.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 2 h
With
4-acetamidobenzenesulfonyl azide; water; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; triethylamine; HATU; potassium hydroxide;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; HATU / N,N-dimethyl-formamide / 20 °C
2: acetic acid / 3 h / 130 °C
3: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 2 h
With
hydrogen; acetic acid; triethylamine; HATU;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; potassium hydroxide / tetrahydrofuran; methanol / 2 h / 70 °C
2: triethylamine; HATU / N,N-dimethyl-formamide / 20 °C
3: acetic acid / 3 h / 130 °C
4: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; methanol / 2 h
With
water; hydrogen; acetic acid; triethylamine; HATU; potassium hydroxide;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;