Z-NH-CO-CO-NH-CO-CO₂Me

Base Information

• Chemical Name: Z-NH-CO-CO-NH-CO-CO₂Me
• CAS No.: 131458-43-0
• Molecular Formula: C₁₃H₁₂N₂O₇
• Molecular Weight: 308.247

Synonyms:Z-NH-CO-CO-NH-CO-CO₂Me

Chemical Property of Z-NH-CO-CO-NH-CO-CO₂Me

Chemical Property:

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Technology Process of Z-NH-CO-CO-NH-CO-CO₂Me

There total 4 articles about Z-NH-CO-CO-NH-CO-CO₂Me which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

Z-Thr-Thr-OMe (83674-34-4) → benzyl (carbamoylcarbonyl)carbamate (131458-44-1) + Z-NH-CO-CO-NH-CO-CO2Me (131458-43-0)

Guidance literature:

With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile; for 1.5h; Ambient temperature; pH 3 phosphate buffer;

DOI:10.1021/ja00003a048

Reference yield: 32.0%

N-(N-benzyloxycarbonyl-L-seryl)-L-serine methyl ester (5874-76-0) → benzyl (carbamoylcarbonyl)carbamate (131458-44-1) + Z-NH-CO-CO-NH-CO-CO2Me (131458-43-0)

Guidance literature:

With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile; for 1.5h; Ambient temperature; pH 3 phosphate buffer;

DOI:10.1021/ja00003a048

Reference yield:

N-(benzyloxycarbonyl)-L-serine (1145-80-8) → Z-NH-CO-CO-NH-CO-CO2Me (131458-43-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / DCC, HOBt

2: NaIO₄, RuCl₃*3H₂O, CH₂N₂ / acetonitrile; CCl₄ / 1.5 h / Ambient temperature; pH 3

With diazomethane; ruthenium trichloride; sodium periodate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrachloromethane; acetonitrile;

DOI:10.1021/ja00094a008

upstream raw materials:

N-(N-benzyloxycarbonyl-L-seryl)-L-serine methyl ester

Z-Thr-Thr-OMe

N-(benzyloxycarbonyl)-L-serine

N-benzyloxycarbonyl-L-treonine

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