trans-1,1-dibenzyloxymethyl-3-(3-t-butyl-3,3-diphenyl-1,1-dimethyldisiloxy)methyl-4-methylcyclopentane

Base Information

Chemical Name:trans-1,1-dibenzyloxymethyl-3-(3-t-butyl-3,3-diphenyl-1,1-dimethyldisiloxy)methyl-4-methylcyclopentane
CAS No.:315191-30-1
Molecular Formula:C₄₁H₅₄O₃Si₂
Molecular Weight:651.049
Hs Code.:

Synonyms:trans-1,1-dibenzyloxymethyl-3-(3-t-butyl-3,3-diphenyl-1,1-dimethyldisiloxy)methyl-4-methylcyclopentane

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Chemical Property of trans-1,1-dibenzyloxymethyl-3-(3-t-butyl-3,3-diphenyl-1,1-dimethyldisiloxy)methyl-4-methylcyclopentane

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Technology Process of trans-1,1-dibenzyloxymethyl-3-(3-t-butyl-3,3-diphenyl-1,1-dimethyldisiloxy)methyl-4-methylcyclopentane

There total 2 articles about trans-1,1-dibenzyloxymethyl-3-(3-t-butyl-3,3-diphenyl-1,1-dimethyldisiloxy)methyl-4-methylcyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 169123-61-9
4,4-bis(benzyloxylmethyl)-1,6-heptadiene

: 315191-15-2
1-tert-butyl-3,3-dimethyl-1,1-diphenyldisiloxane

: 1-((1R,2R)-4,4-Bis-benzyloxymethyl-2-methyl-cyclopentylmethyl)-3-tert-butyl-1,1-dimethyl-3,3-diphenyl-disiloxane

: 315191-30-1
trans-1,1-dibenzyloxymethyl-3-(3-t-butyl-3,3-diphenyl-1,1-dimethyldisiloxy)methyl-4-methylcyclopentane

Guidance literature:: With [(R)-(+)-4-isopropyl-2-(2-pyridinyl)-2-oxazoline]Pd(Me)Cl; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In dichloromethane; at -20 ℃; for 12h; Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)01321-6

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 315191-30-1
trans-1,1-dibenzyloxymethyl-3-(3-t-butyl-3,3-diphenyl-1,1-dimethyldisiloxy)methyl-4-methylcyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaHCO₃ / H₂O; tetrahydrofuran / 0 - 20 °C

2: [(R)-(+)-4-isopropyl-2-(2-pyridinyl)-2-oxazoline]Pd(Me)Cl; NaB[3,5-C₆H₃(CF₃)2]4 / CH₂Cl₂ / 12 h / -20 °C

With [(R)-(+)-4-isopropyl-2-(2-pyridinyl)-2-oxazoline]Pd(Me)Cl; sodium hydrogencarbonate; sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jo015724n