8-desoxy-isocaespitol

Base Information

Chemical Name:8-desoxy-isocaespitol
CAS No.:74323-44-7
Molecular Formula:C₁₅H₂₅Br₂ClO
Molecular Weight:416.624
Hs Code.:

Synonyms:8-desoxy-isocaespitol

Suppliers and Price of 8-desoxy-isocaespitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-desoxy-isocaespitol

Chemical Property:

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Technology Process of 8-desoxy-isocaespitol

There total 3 articles about 8-desoxy-isocaespitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 74323-45-8,74364-61-7
(3R,6S)-3-Bromo-2,2,6-trimethyl-6-((S)-4-methyl-cyclohex-3-enyl)-tetrahydro-pyran

: 74323-48-1,124264-63-7
(3R,6S)-3-Bromo-6-((1S,3R,4R)-3-bromo-4-chloro-4-methyl-cyclohexyl)-2,2,6-trimethyl-tetrahydro-pyran

: 74323-44-7,74364-62-8
(+/-)-8-desoxy-isocaespitol

Guidance literature:: With bromine chloride; at -78 ℃; Title compound not separated from byproducts;
DOI:10.1016/S0040-4039(00)71409-2

Reference yield:

: 29548-30-9
farnesyl acetate

: 74323-44-7,74364-62-8
(+/-)-8-desoxy-isocaespitol

Guidance literature:: Multi-step reaction with 3 steps

1: N-bromosuccinimide / H₂O; tetrahydrofuran

2: 9 percent / LiClO₄*3H₂O / acetic acid; acetic anhydride / 48 h / Ambient temperature

3: 18 percent / bromine chloride / -78 °C

With N-Bromosuccinimide; lithium perchlorate; bromine chloride; In tetrahydrofuran; water; acetic anhydride; acetic acid;
DOI:10.1016/S0040-4039(00)71409-2

Reference yield:

: 74323-46-9
Acetic acid (2E,6E)-10-bromo-11-hydroxy-3,7,11-trimethyl-dodeca-2,6-dienyl ester

: 74323-44-7,74364-62-8
(+/-)-8-desoxy-isocaespitol

Guidance literature:: Multi-step reaction with 2 steps

1: 9 percent / LiClO₄*3H₂O / acetic acid; acetic anhydride / 48 h / Ambient temperature

2: 18 percent / bromine chloride / -78 °C

With lithium perchlorate; bromine chloride; In acetic anhydride; acetic acid;
DOI:10.1016/S0040-4039(00)71409-2