7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one

Base Information

Chemical Name:7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one
CAS No.:116211-75-7
Molecular Formula:C₁₇H₁₈Cl₂O₅
Molecular Weight:373.233
Hs Code.:

Synonyms:7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one

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Chemical Property of 7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one

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Technology Process of 7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one

There total 5 articles about 7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 116211-72-4
7,7-dichloro-3-hydroxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one

: 77-78-1
dimethyl sulfate

: 116211-75-7
7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one

Guidance literature:: With potassium carbonate; In acetone; for 4h; Ambient temperature;
DOI:10.1021/jo00256a009

Reference yield:

: 116211-74-6
(1α,3α,6α)-7,7-dichloro-3-hydroxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>heptan-2-one

: 116211-75-7
7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / trifluoroacetic anhydride (TFAA), DMSO / CH₂Cl₂ / 2 h / -60 °C

2: 87 percent / K₂CO₃ / acetone / 4 h / Ambient temperature

With potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride; In dichloromethane; acetone;
DOI:10.1021/jo00256a009

Reference yield:

: 116211-63-3
trans-4-(2',3',4'-trimethoxyphenyl)cyclohex-3-ene-1,2-diol

: 116211-75-7
7,7-dichloro-3-methoxy-6-(2',3',4'-trimethoxyphenyl)bicyclo<4.1.0>hept-3-en-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / pyridine / 20 h / Ambient temperature

3: 87 percent / K₂CO₃ / acetone / 4 h / Ambient temperature

With pyridine; potassium carbonate; In acetone;
DOI:10.1021/jo00256a009