2-[(4-ethoxyphenyl)imino]-5-methyl-1,3-di(tert-butoxycarbonyl)imidazolidine

Base Information

Chemical Name:2-[(4-ethoxyphenyl)imino]-5-methyl-1,3-di(tert-butoxycarbonyl)imidazolidine
CAS No.:1393670-37-5
Molecular Formula:C₂₂H₃₃N₃O₅
Molecular Weight:419.521
Hs Code.:

Synonyms:2-[(4-ethoxyphenyl)imino]-5-methyl-1,3-di(tert-butoxycarbonyl)imidazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(4-ethoxyphenyl)imino]-5-methyl-1,3-di(tert-butoxycarbonyl)imidazolidine

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Technology Process of 2-[(4-ethoxyphenyl)imino]-5-methyl-1,3-di(tert-butoxycarbonyl)imidazolidine

There total 2 articles about 2-[(4-ethoxyphenyl)imino]-5-methyl-1,3-di(tert-butoxycarbonyl)imidazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1393670-62-6
1,3-di(tert-butoxycarbonyl)-4-methylimidazolidine-2-thione

: 156-43-4
4-Ethoxyaniline

: 1393670-37-5
2-[(4-ethoxyphenyl)imino]-5-methyl-1,3-di(tert-butoxycarbonyl)imidazolidine

Guidance literature:: With triethylamine; mercury dichloride; In dichloromethane; at 0 - 20 ℃; for 17h;
DOI:10.1016/j.tetlet.2012.06.042

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1393670-37-5
2-[(4-ethoxyphenyl)imino]-5-methyl-1,3-di(tert-butoxycarbonyl)imidazolidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h

1.2: 2.5 h

2.1: mercury dichloride; triethylamine / dichloromethane / 15 h / 0 - 20 °C

With sodium hydride; triethylamine; mercury dichloride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1016/j.ejmech.2014.05.057