carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

Base Information

Chemical Name:carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester
CAS No.:1196064-27-3
Molecular Formula:C₄₄H₆₃NO₆Si₂
Molecular Weight:758.158
Hs Code.:

Synonyms:carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

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Technology Process of carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

There total 1 articles about carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1196064-26-2
carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

: 21047-57-4
diethyl (1-diazo-2-oxopropyl)phosphonate

: 1196064-27-3
carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1055/s-0029-1216921

Reference yield: 98.0%

: 1196064-27-3
carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

: 1196064-28-4
carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-hydroxynon-3-enyl ester

Guidance literature:: With water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 6h;
DOI:10.1055/s-0029-1216921

Reference yield: 92.0%

: 1196064-27-3
carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-but-3-ynyl-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

: 1196064-31-9
carbamic acid (1S,2S,3E,5S)-1-but-3-enyl-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

Guidance literature:: With quinoline; Lindlar's catalyst; hydrogen; cyclohexene; In acetone; cyclohexene; for 8h; Inert atmosphere;
DOI:10.1055/s-0029-1216921