Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester

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Chemical Name:Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester
CAS No.:202057-89-4
Molecular Formula:C₂₇H₃₀N₂O₆
Molecular Weight:478.545
Hs Code.:

Synonyms:Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester

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Chemical Property of Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester

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Technology Process of Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester

There total 9 articles about Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 108-24-7
acetic anhydride

: 202058-01-3
2,8-bis(2-hydroxyethyl)-3,7-dimethyl-5-phenyl-1,9-diformyldipyrrylmethane

: 202057-89-4
Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester

Guidance literature:: In pyridine; at 25 ℃; for 2h;
DOI:10.1021/jo971807l

Reference yield:

: 87281-59-2
4-Methoxycarbonylmethyl-3-methyl-5-trichloromethyl-1H-pyrrole-2-carboxylic acid benzyl ester

: 202057-89-4
Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: NaOAc / 72 h / 50 °C

2: 68 percent / H₂ / Pd/C / ethanol / 2 h

3: 97 percent / I₂, KI, NaHCO₃ / ethanol; H₂O / 1 h / Heating

4: 74 percent / H₂, NaOAc / Pd/C / methanol / 2 h / 2585.7 Torr

5: 80 percent / p-TsOH / CHCl₃ / 2 h / Heating

6: 66 percent / B₂H₆ / tetrahydrofuran / 26 h / 25 °C

7: 74 percent / KOH / ethanol; H₂O / 110 °C

8: 51 percent / TMOF / trifluoroacetic acid / 0.25 h / 0 - 5 °C

9: 66 percent / pyridine / 2 h / 25 °C

With potassium hydroxide; hydrogen; iodine; sodium acetate; sodium hydrogencarbonate; toluene-4-sulfonic acid; potassium iodide; diborane; trimethyl orthoformate; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; ethanol; chloroform; water; trifluoroacetic acid;
DOI:10.1021/jo971807l

Reference yield:

: 202057-95-2
3-Methoxycarbonylmethyl-4-methyl-1H-pyrrole-2,5-dicarboxylic acid 2-methyl ester

: 202057-89-4
Acetic acid 2-(5-{[4-(2-acetoxy-ethyl)-5-formyl-3-methyl-1H-pyrrol-2-yl]-phenyl-methyl}-2-formyl-4-methyl-1H-pyrrol-3-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 97 percent / I₂, KI, NaHCO₃ / ethanol; H₂O / 1 h / Heating

2: 74 percent / H₂, NaOAc / Pd/C / methanol / 2 h / 2585.7 Torr

3: 80 percent / p-TsOH / CHCl₃ / 2 h / Heating

4: 66 percent / B₂H₆ / tetrahydrofuran / 26 h / 25 °C

5: 74 percent / KOH / ethanol; H₂O / 110 °C

6: 51 percent / TMOF / trifluoroacetic acid / 0.25 h / 0 - 5 °C

7: 66 percent / pyridine / 2 h / 25 °C

With potassium hydroxide; hydrogen; iodine; sodium acetate; sodium hydrogencarbonate; toluene-4-sulfonic acid; potassium iodide; diborane; trimethyl orthoformate; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; ethanol; chloroform; water; trifluoroacetic acid;
DOI:10.1021/jo971807l