2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester

Base Information

Chemical Name:2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester
CAS No.:158835-89-3
Molecular Formula:C₂₁H₂₇N₃O₆
Molecular Weight:417.462
Hs Code.:

Synonyms:2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester

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Chemical Property of 2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester

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Technology Process of 2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester

There total 4 articles about 2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 184001-57-8
N-[2-(3,4-dimethoxyphenyl)ethyl]-N-hex-5-enoylmalonamic acid ethyl ester

: 158835-89-3
2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester

Guidance literature:: With triethylamine; Methanesulfonyl azide; In acetonitrile; for 3h; Ambient temperature;
DOI:10.1021/jo9607267

Reference yield:

: 1577-22-6
5-hexenoic acid

: 158835-89-3
2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1,1'-carbonyldiimidazole / 1.) CH₂Cl₂, room temp., 2 h, 2.) CH₂Cl₂, 25 deg C, 10 h

2: 78 percent / benzene / 1 h / Heating

3: 95 percent / mesyl azide, Et₃N / acetonitrile / 3 h / Ambient temperature

With triethylamine; Methanesulfonyl azide; 1,1'-carbonyldiimidazole; In acetonitrile; benzene;
DOI:10.1021/jo9607267

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 158835-89-3
2-diazo-N-<2-(3,4-dimethoxyphenyl)ethyl>-N-hex-5-enoylmalonamic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1,1'-carbonyldiimidazole / 1.) CH₂Cl₂, room temp., 2 h, 2.) CH₂Cl₂, 25 deg C, 10 h

2: 78 percent / benzene / 1 h / Heating

3: 95 percent / mesyl azide, Et₃N / acetonitrile / 3 h / Ambient temperature

With triethylamine; Methanesulfonyl azide; 1,1'-carbonyldiimidazole; In acetonitrile; benzene;
DOI:10.1021/jo9607267