C₃₃H₅₆O₆Si₂

Base Information

Chemical Name:C₃₃H₅₆O₆Si₂
CAS No.:1268455-87-3
Molecular Formula:C₃₃H₅₆O₆Si₂
Molecular Weight:604.975
Hs Code.:

C<sub>33</sub>H<sub>56</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₃₃H₅₆O₆Si₂

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Chemical Property of C₃₃H₅₆O₆Si₂

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Technology Process of C₃₃H₅₆O₆Si₂

There total 24 articles about C₃₃H₅₆O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1268455-99-7
C₃₃H₅₆O₅Si₂

: 1268455-87-3
C₃₃H₅₆O₆Si₂

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 0 - 20 ℃;
DOI:10.1021/ol1031409

Reference yield:

: 1268455-52-2
C₂₄H₃₈O₄Si

: 1268455-87-3
C₃₃H₅₆O₆Si₂

Guidance literature:: Multi-step reaction with 14 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: methanol; camphor-10-sulfonic acid / dichloromethane / 12 h / 20 °C

4.1: 1H-imidazole / N,N-dimethyl-formamide / 14.5 h / 50 °C

5.1: methanol; camphor-10-sulfonic acid / dichloromethane / 2 h / 0 °C

6.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 0.5 h / 0 °C

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 20 °C

8.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

9.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; hexamethyldistannane; lithium chloride / tetrahydrofuran / 1.5 h / 70 °C

9.2: 3.5 h / 20 °C

10.1: zinc borohydride / diethyl ether / 24 h / -40 °C

11.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C

12.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 - 20 °C / pH 7 / aq. buffer

13.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 6 h / 0 °C

14.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0 - 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; methanol; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-methyl-but-2-ene; zinc borohydride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hexamethyldistannane; sulfur trioxide pyridine complex; sodium hydride; triethylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil; tert-butyl alcohol;
DOI:10.1021/ol1031409

Reference yield:

: C₂₁H₃₂O₄Si

: 1268455-87-3
C₃₃H₅₆O₆Si₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1.5 h / 20 °C

2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0 - 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; hexamethyldistannane; lithium chloride / tetrahydrofuran / 1.5 h / 70 °C

3.2: 3.5 h / 20 °C

4.1: zinc borohydride / diethyl ether / 24 h / -40 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 0.25 h / 0 °C

6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 - 20 °C / pH 7 / aq. buffer

7.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 6 h / 0 °C

8.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0 - 20 °C

With 2,6-dimethylpyridine; dmap; sodium chlorite; sodium dihydrogenphosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2-methyl-but-2-ene; zinc borohydride; hexamethyldistannane; sulfur trioxide pyridine complex; triethylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium chloride; In tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide; tert-butyl alcohol;
DOI:10.1021/ol1031409