Technology Process of C28H44IN3O5
There total 11 articles about C28H44IN3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1.1: benzene / 3 h / Heating / reflux
2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
2.2: 2 h
3.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C
4.1: trimethylaluminum / dichloromethane; toluene / 0.21 h
4.2: 24 h
4.3: 2 h
5.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 h
6.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 1 h / 0 - 20 °C
7.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 3 h
8.1: periodic acid / tetrahydrofuran; water / 12 h
9.1: sodium cyanoborohydride; acetic acid / methanol; water / 12 h
With
titanium(IV) isopropylate; osmium(VIII) oxide; trimethylaluminum; sodium cyanoborohydride; potassium carbonate; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; periodic acid; trifluoroacetic acid;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
1.2: 2 h
2.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C
3.1: trimethylaluminum / dichloromethane; toluene / 0.21 h
3.2: 24 h
3.3: 2 h
4.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 h
5.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 1 h / 0 - 20 °C
6.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 3 h
7.1: periodic acid / tetrahydrofuran; water / 12 h
8.1: sodium cyanoborohydride; acetic acid / methanol; water / 12 h
With
titanium(IV) isopropylate; osmium(VIII) oxide; trimethylaluminum; sodium cyanoborohydride; potassium carbonate; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; periodic acid; trifluoroacetic acid;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
- Guidance literature:
-
Multi-step reaction with 10 steps
1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 18 h / pH 3
1.2: pH 7 / Alkaline aqueous solution
2.1: benzene / 3 h / Heating / reflux
3.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation
3.2: 2 h
4.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 °C
5.1: trimethylaluminum / dichloromethane; toluene / 0.21 h
5.2: 24 h
5.3: 2 h
6.1: potassium carbonate / N,N-dimethyl-formamide / 2.5 h
7.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 1 h / 0 - 20 °C
8.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 3 h
9.1: periodic acid / tetrahydrofuran; water / 12 h
10.1: sodium cyanoborohydride; acetic acid / methanol; water / 12 h
With
titanium(IV) isopropylate; hydrogenchloride; osmium(VIII) oxide; methyl orange; trimethylaluminum; sodium cyanoborohydride; potassium carbonate; pyridine hydrogenfluoride; acetic acid; 4-methylmorpholine N-oxide; periodic acid; trifluoroacetic acid;
In
tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; benzene;
