N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide

Base Information

• Chemical Name: N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide
• CAS No.: 300854-53-9
• Molecular Formula: C₂₂H₂₅N₅O₇
• Molecular Weight: 471.47

Synonyms:N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide

Chemical Property of N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide

Chemical Property:

Purity/Quality:

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Technology Process of N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide

There total 2 articles about N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-(2-{acetyl-[2-(acetyl-phenyl-amino)-ethyl]-amino}-ethyl)-N-phenyl-acetamide (300854-52-8) → N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide (300854-53-9)

Guidance literature:

With sulfuric acid; nitric acid; In acetic acid; at 20 ℃; for 48h;

DOI:10.1055/s-2000-6421

Reference yield:

bis(2-phenylaminoethyl)amine (4432-90-0) → N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide (300854-53-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 63 percent / 2 h / Heating

2: 100 percent / HNO₃; H₂SO₄ / acetic acid / 48 h / 20 °C

With sulfuric acid; nitric acid; In acetic acid; 1: Acetylation / 2: Nitration;

DOI:10.1055/s-2000-6421

Reference yield: 57.0%

N-[2-(acetyl-{2-[acetyl-(4-nitro-phenyl)-amino]-ethyl}-amino)-ethyl]-N-(4-nitro-phenyl)-acetamide (300854-53-9) → N-(4-nitrophenyl)-N-[2-({2-[(4-nitrophenyl)amino]ethyl}-amino)ethyl]amine (300854-47-1)

Guidance literature:

With hydrogenchloride; for 1h; Heating;

DOI:10.1055/s-2000-6421

upstream raw materials:

N-(2-{acetyl-[2-(acetyl-phenyl-amino)-ethyl]-amino}-ethyl)-N-phenyl-acetamide

bis(2-phenylaminoethyl)amine

Downstream raw materials:

N-(4-nitrophenyl)-N-[2-({2-[(4-nitrophenyl)amino]ethyl}-amino)ethyl]amine

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