Technology Process of C23H29NO2
There total 5 articles about C23H29NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
tetrahydrofuran;
for 19h;
Heating;
DOI:10.1021/jm010992z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-BuLi / hexane; tetrahydrofuran / 0.08 h / -78 °C
1.2: 39 percent / hexane; tetrahydrofuran / 5 h / -78 - 20 °C
2.1: 86 percent / p-toluenesulfonic acid monohydrate / methanol / 96 h / 20 °C
3.1: 70 percent / ammonium formate / 10percent Pd/C / methanol / 2.5 h / Heating
4.1: 64 percent / K2CO3 / tetrahydrofuran / 19 h / Heating
With
n-butyllithium; ammonium formate; potassium carbonate; toluene-4-sulfonic acid;
10percent Pd/C;
In
tetrahydrofuran; methanol; hexane;
DOI:10.1021/jm010992z
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-BuLi / hexane; tetrahydrofuran / 0.08 h / -78 °C
1.2: 39 percent / hexane; tetrahydrofuran / 5 h / -78 - 20 °C
2.1: 86 percent / p-toluenesulfonic acid monohydrate / methanol / 96 h / 20 °C
3.1: 70 percent / ammonium formate / 10percent Pd/C / methanol / 2.5 h / Heating
4.1: 64 percent / K2CO3 / tetrahydrofuran / 19 h / Heating
With
n-butyllithium; ammonium formate; potassium carbonate; toluene-4-sulfonic acid;
10percent Pd/C;
In
tetrahydrofuran; methanol; hexane;
DOI:10.1021/jm010992z
